GCMS analysis results for sample AE00106, Feb 2002

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Laboratory report listing unknown compounds and surrogate recovery for sample AE00106 analyzed on February 7, 2002.

NYC-WTC_000050774–000050792

Folder label: “GCMS X 1/4/02 A 1/25/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\O2 JAN25\00106.D Vial: 5 . Acq On : 25 Jan 2002 1:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 9 Cyclopentasiloxane, decamet... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 12.54 0.07 ug/L 44730 Naphthalene-d8 13.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 72 2 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 53 3 M-HYDROXYPHENETHANOL 2TMS 282 C14H2602Si2 000000-00-0 25 4 Methyl 5-[ [5'-nitro-3'-(1",.. 532 C19H12N6O9S2 000000-00-0 9 Abundance Scan 803 (12.541 min): 00106.D (■) m/ z 73.10 100.00% 73

5000 267 I-1 45 12.20 12.40 12.60 12.80 P • i • ■ ■ • i • ■ ■ ■ i ■ ■ ■ ’ i • • • • i ■ ■ ■ ■ i ■ ■ ■ ■ i • • ■ ■ i ■ ■ • • i ■ - m/z 267.00 33.63% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 i-1 12.20 12.40 12.60 12.80 m/z 355.10 26.82% 323339 | ■ i ■ • ■ ■ 191207 2511 i ■'' ■ r ' ■ ■ i ■ ■ ■ ■ i ‘ 1‘I "TTTT I ’'' • I '''' 'l' ' •" I'

n/Z“> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 Til 12.20 12.40 12.60 12.80 5000 267 m/z 268.10 11.09% 355 45 1 193 223 251 323339 TT‘ T 11TOLTCTWTT1TTIWTTTTTT 11111111111" 1111 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #227925: M-HYDROXYPHENETHANOL 2TMS • ' i ■ ■ ' ' i ■ ■ l ■ • ■ ■ l • ■ • ■ I • 73 12.20 12.40 12.60 12.80 m/z 356.10 10.77% 103 5000 267 —282

n/z--> 47 — l... '' I'''' I 126 147 177193 ...... 1...... I........ ^■■^■1 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 249 i ■ ■ ■ ■ । ■•■ •। ■ • ■ •। T‘ 1 1 Tr' ' ' I ' ' i • • • • । 12.20 12.40 12.60 12.80 • i ■

30106.D SCAN508.M Mon Jan 28 09:49:54 2002 Page 11

NYC-WTC_000050788

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NYC-WTC_000050788Source: NYC Law Department, mirrored locally

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