GCMS results for sample AE00557, Jan 17 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00557 showing surrogate recovery and unknown compounds detected on January 17, 2002.

NYC-WTC_000051768–000051781

Folder label: “GCMS X 1/9/02 A 1/15/02”

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NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02JAN15\00557.D Vial: 1 Acq On : 15 Jan 2002 1:32 pm Operator: • Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 7 9H-Carbazole (CAS) $$ Carba... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 23.42 0.20 ug/L 114236 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 9H-Carbazole (CAS) $$ Carbazole ... 167 C12H9N 000086-74-8 91 2 D-Galactitol, 2-(acetylmethylami. .. 363 C16H29NO8 074410-42-7 90 3 Carbazole 167 C12H9N 000086-74-8 87 4 Carbazole 167 C12H9N 000086-74-8 87 Abundance Scan 1756 (23.422 min): 00557. D (-) m/z 167.10 100.00% 167

5000

_ 83 139 I‘I"I r1 1 1 1 r' 1 23.00 23.20 23.40 23.60 23.80 o1Tt 40 51,62,14113.. .4 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 188 1 ■ ।11 ■ ■ । ■ ■' ■ । ■ ■ ■ ■ ।■11 । ■ ■ ■ ■ । ■ ■ ■ ■ । ■1 ■ । ■ m/z 166.10 17.61% Abundance #69297:9H-Carbazole (CAS) $$ Carbazole $$ 9-Azafluorene $... 167

5000 23.00 23.20 23.40 23.60 23.80 m/ z 83.60 13.73% 83 139 i, 0 _8 ■ ■ i ■ ■ ■ ‘ ■ ■ ■ i n ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■' i ■'' ■ i''

/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #308428: D-Galactitol, 2-(acetylmethylamino)-2-deoxy-3,4,6... 167 -AAAAAAAAAAL 23.00 23.20 23.40 23.60 23.80 5000 m/z 168.10 13.57%

83 ... 139 62 L 113 |i 327 343 o1TPU10 i ' ' । ■ ■ ■ ■T■ Tf ■' i ■1 ■11' •'11 ■'1' i'' ■ ■ i ■ ■'' i ■1111'111 r ' ■r i1 ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #69295: Carbazole /I+d*I‘IY‘U‘I‘TEM‘H 167 23.00 23.20 23.40 23.60 23.80 m/z 139.10 11.65%

5000

44 — _ 139

m/z-> 0 40 60 89 TTT 80 +13. .4, ----- 100 120 140 160 180 200 220 240 260 280 300 320 340 ‘ i111 1 r1 1 23.00 23.20 23.40 23.60 23.80

30557.D SCAN508.M Wed Jan 16 08:13:58 2002 Page 9

NYC-WTC_000051780

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