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GCMS surrogate recovery results for sample AE00317, Jan 2002

Machine-extracted title · confidence 90%

Laboratory record documenting GCMS surrogate recovery data for sample AE00317 analyzed on January 10, 2002.

NYC-WTC_000050977–000050993

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050991
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\O2 JAN10\00317 . D Vial: 4 Acq On : 10 Jan 2002 10:57 am Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 9H-Carbazole (CAS) $$ Carba... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 23.42 0.13 ug/L 70576 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 9H-Carbazole (CAS) $$ Carbazole ... 167 C12H9N 000086-74-8 90 2 9H-Carbazole)(CAS) $$ Carbazole ... 167 C12H9N 000086-74-8 90 3 Carbazole $$9H-Carbazole $$ Dib... 167 C12H9N 000086-74-8 86 4 Carbazole 167 C12H9N 000086-74-8 86 Abundance Scan 1756 (23.422 min): 00317.D (-) m/z 167.10 100.00% 167

5000

83 139 11.7 51 63 69 113 23.00 23.20 23.40 23.60 23.80 I 0 ।1 ■ ■ • ।r 1' ■11111 ll rh............+ 1 i ' 1 ■ I ■ ■ ■ ■ ।' ■ ■ ■ । ■ ■ ■ • । ■ ■ • ■ ।'1'11111111 m/z 166.00 18.80% n/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #69299:9H-Carbazole (CAS) $$ Carbazole $$ 9-Azafluorene $... 1$7

5000 2300 23.20 23.40 23.60 23.80 84 m/z 168.10 15.35% 63 70 _______ 0 T"TTTIITTTTTTTTTTT Tini n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #69297:9H-Carbazole (CAS) $$ Carbazole $$ 9-Azafluorene $... 167 ----- 23.00 23.20 23.40 23.60 23.80 5000 m/ Z 83.50 12.89%

83 139 1 98 113 || 0'| । 11 ' । 1 । 11 । 1 1 111 ' 1;-mPPPITIPTTTH /z-> Abundance 40 50 60 70 80 90 100 110 120 130 140 150 160 170 #69293: Carbazole $$ 9H-Carbazole $$ Dibenzopyrrole $$ Dib... 167 IAAALAALAAAAAAAAAAAAAl 23.00 23.20 23.40 23.60 23.80 m/z 139.00 12.77%

5000

84 139

/z-> O-T 40 ■ i ' ' ' ' i ■ ' ■ ■ i ■ 50 60 70 J.. 12... . 80 90 < 11 ■ ■ ■ ■ । • । f 11 > 100 110 120 130 140 150 160 170 23.00 23.20 23.40 23.60 23.80

)0317.D SCAN508.M Thu Jan 10 11:52:17 2002 Page 10

NYC-WTC_000050991

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NYC-WTC_000050991Source: NYC Law Department, mirrored locally

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