GCMS blank analysis for sample AE00365, Jan-Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\0109B.D Vial: 1 Acq On : 15 Jan 2002 10:12 am Operator: ' Sample : lab blank 1/9 Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 5 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 22.77 0.36 ug/L 180697 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 86 2 Phenanthrene-dlO 188 C14D10 001517-22-2 64 3 1-methyl-5-methoxy-1,4-epoxynaph... 188 C12H1202 000000-00-0 59 4 Anthracene-dlO- 188 C14D10 001719-06-8 56 Abundance Scan 1699 (22.771 min): 0109B.D (-) m/z 188.10 100.00% 188

5000

94 66 80 ............................. 132 158 22.40 22.60 22.80 23.00 23.20 01 ■ i111 ■ i11 ‘ U1111 j 111 — -p-r m/z 94.00 20.16% m/z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

- 5000- 22.40 22.60 22.80 23.00 23.20 80 94 m/z 189.10 11.42% 66 158 01 H ■ Tr. IT ooutt ■ ■ i ■ ■ ' ' i ■ ■ ■ ' i 1 1 ' ■ i' ' ' ' i I 1 111| < <11 I > > 111111111111 n/z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 184.10 10.22%

80 94 160 66

miz-> Of 111111111 60 70 80 90 100 110 120 130 140 150 160 170 180 190 — ... wi... Abundance #98101:1 -methyl-5-methoxy-1,4-epoxynaphthalene --------------------------- 188 22.40 22.60 22.80 23.00 23.20 115 m/z 158.05 9.24% 145 173 A 5000 127 160

0 ■ I " ■ 11 11' 11 < I । >1 111 " < 11 |l, । 1 1 1 ....... Il..... I l1 - m/z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

0109B.D SCAN508.M Wed Jan 16 08:14:17 2002 Page 7

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