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GCMS surrogate recovery results for sample AE00280, Jan 2002

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Laboratory record documenting GCMS surrogate recovery data for sample AE00280 analyzed on January 10, 2002.

NYC-WTC_000050893–000050911

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050907
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\O2JAN09\280.D vial: 5 Acq On 9 Jan 2002 9:31 pm Operator: • Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 8 2-Propanol, 1-(2-methoxypro... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

9.85 0.20 ug/L 103260 1,4-Dichlorobenzene-d4 9.72

.it# of 5 Tentative ID MW MolForm CAS# Qual -Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 83 PROPYLENE GLYCOL TRIMER 1 174 C9H18O3 000000-00-0 78 3 Butane, 2-methoxy- (CAS) $$ Meth... 88 C5H120 006795-87-5 40 4 3-Hexanol 102 C6H140 000623-37-0 39 Abundance Scan 567 (9.847 min): 280.D (-) m/ z 59.10 100.00% 50

5000

45 M) 73 104 9.60 9.80 10.00 10.20

•n/z--> 0'1 i 1 ' ' ' I ' 10 20 — 30 40 50 60 + , l J..............■,. । 70 80 . ................ 90 100 110 120 130 m/z 45.10 11.54% Abundance #43942:2-Propanol, 1-(2-methoxypropoxy)- $$ 1-(2-Methoxyp... 59

5000 ......... 1..... 9.60 9.80 10.00 10.20 m/z 41.00 10.73% 31 45 o1 'I'■'' I' ' ' ' I I ' 1... 7.7r....... 194.....11130

W/n A 1 ........ . 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #78532: PROPYLENE GLYCOL TRIMER 1 59 L 9.60 9.80 10.00 10.20 5000 41 m/z 73.10 10.15% 103

0—T ■ i > ■ > • i ■ 4 73 87 117 130 .. ................ . 1I99IB—TTT 1 11 11 1 111 1 1 1 ' I' /z-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 #4937: Butane, 2-methoxy- (CAS) $$ Methyl sec-butyl ether... 59 A9.60 \ TT 9.80 ( 11 10.00 10.20 m/z43.10 9.81%

5000

15 27 W 45 .73 0 ...... .............. . I ' I ' '''I' ' 1 ' I' ' ' ' I ' ‘ ‘I" iJl...... ।...... ....................... ...... n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 9.60 9.80 10.00 10.20

280.D SCAN508.M Thu Jan 10 11:51:55 2002 Page 10

NYC-WTC_000050907

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NYC-WTC_000050907Source: NYC Law Department, mirrored locally

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