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GCMS analysis results for sample AE00613, Feb 2002

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Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.

NYC-WTC_000051586–000051604

Folder label: “GCMS X 1/9/02 A 1/29/02

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Scanned page image, NYC-WTC_000051602
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN29\00613 .D Vial: 2 Acq On : 29 Jan 2002 3:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : J anuary 2 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.36 ug/L 304745 Phenanthrene-dl0 22.65 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Anthracene-D10 188 C14D10 000000-00-0 91 3 Anthracene-diO- 188 C14D10 001719-06-8 91 4 Phenanthrene-diO 188 C14D10 001517-22-2 91 Abundance Scan 1699 (22.771 min): 00613.D (-) m/z 188.10 100.00% 188

5000

80 94 132 146 160 22.40 22.60 22.80 23.00 23.20 HPHL fumn 42 54 66 /z-> m WTTTTTT +— ++ i1 ■ ■' i1 ■'' । 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 189.10 16.83% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/ Z 80.10 15.50% ......................... 66 . — 158 1 h'1"" | I I I I | I I I I ( I m-1 I ! I I | . I ! I | | I > > | TT I I | I r IT| I

/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D10 188

22.40 22.60 22.80 23.00 23.20 5000 m/ z 94.05 14.43% 80 94 66 160 ----- ' I " " I ' 1 " I ' " ' I 1 mrpi I I I |-TI I I | I I I V| I I ! I | I 1' " 11 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- "I r . , 1T* IDIttrI . r I , 188 22.40 22,60 22.80 23.00 23.20 m/z 184.10 12.65%

5000

66 80 94 160 TITTTTTTTTmWTTTTIIWIIPIPPTT 180 4—. mfa-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

3613.D SCAN508.M Wed Jan 30 09:02:10 2002 Page 13

NYC-WTC_000051602

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NYC-WTC_000051602Source: NYC Law Department, mirrored locally

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