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GCMS analysis results for sample AE00613, Feb 2002

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Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.

NYC-WTC_000051586–000051604

Folder label: “GCMS X 1/9/02 A 1/29/02

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NYC 9/11 Public Portal Document

—X

Data File : C:\MSDCHEM\1\5973N\02JAN29\00613.D vial: 2 • Acq On : 29 Jan 2002 3:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise 2002: January 29, Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 12 1,2-Benzenedicarboxylic aci... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 24.85 0.15 ug/L 123585 Phenanthrene -dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, bu... 278 C16H2204 017851-53-5 90 2 1,2-Benzenedicarboxylic acid, bi ... 278 C16H2204 000084-69-5 83 3 1,2-Benzenedicarboxylic acid, bu... 334 C20H30O4 000085-69-8 83 4 1,2-Benzenedicarboxylic acid, bu... 304 C18H2404 000084-64-0 83 Abundance Scan 1881 (24.849 min): 00613. D (-) m/z 149.00 100.00% 149

5000

TTTT 41 57 76 93 121 205 223 24.60 24.80 25.00 25.20 ----- TVTIIPaT ■ । ■ ■ ■1111 ■' i ■' ■ ■ i11'111 m/Z 150.00 9.53% /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #223230:1,2-Benzenedicarboxylic acid, butyl 2-methylpropy... 149

5000 24 60 24.80 25.00 25.20 m/ z 41.10 7.77% 41 57 76 104 205 223 -- 121 278 ‘I""-I0-E‘TN‘TT‘I‘‘‘"T‘TVT‘‘‘‘G"ITUTTTTTTTTT‘‘‘‘1‘11177 Wz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #223251:1,2-Benzenedicarboxylic acid, bis(2-methylpropyl)... 149 I ' ’ ' I ' 24.60 24.80 25.00 25.20 5000 m/z57.10 5.53%

57 1,76 104 121......167........205 223 T ‘001u ir ■ ■' i' • > t I > ' ' r । 278 —0‘u——nnd3 । r i . . । . . < > । > r. , । r, . , । , i । । r> ' 1 I 1 1 ' /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 -- Abundance #284879:1,2-Benzenedicarboxylic acid, butyl 2-ethylhexyl ... 149 24,60 24.80 25.00 25.20 m/z 56.10 5.12%

5000

57 76 104 121 205 223 TTTTTPT ‘ 111110110UTU-U-TTT‘TT‘261 279 334 1m1‘1"‘T"‘TOUTT m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 24.60 24.80 25.00 25.20

)0613.D SCAN508.M Wed Jan 30 09:02:10 2002 Page 14

NYC-WTC_000051603

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NYC-WTC_000051603Source: NYC Law Department, mirrored locally

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