GCMS DFTPP calibration report, Feb 5 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB05\29232A.D Vial: 4 Acq On 5 Feb 2002 1:13 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508-M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ***************************** * * * * * *********************************** Peak Number 13 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.39 ug/L 486649 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Anthracene-D10 188 C14D10 000000-00-0 87 3 Phenanthrene-diO 188 C14D10 001517-22-2 62 4 Anthracene-diO- 188 C14D10 001719-06-8 62 Abundance Scan 1699 (22,771 min): 29232A.D (-) m/z 188.10 100.00% 188

5000

80 94 ... r 22.40 22.60 22.80 23.00 23.20

n/z-> 0- 44 54 1-1111111411801) 40 66 । 102 —-mmpp 132 „146 44.10— 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 m/z 94.10 19.70% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

- 5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z 80-10 13.17% 66 158— 0- ' i' ■1 ■ i ■ ■ ■11 ■'1 ■ i ■ TTIt 0000000002100021002210111/0001111 m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D10 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 184.10 11.96% 80 94 66 160 01 mm mH miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 ............ —...................... , 188 22.40 22.60 22.80 23.00 23.20 m/z 189.10 11.36% A 5000

80 94 160

m/z-> 0 66 ■ ■ i ■ ■ ‘ ■ i " 111"'11" -------- 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ... w... -- 22.40 22.60 22.80 23.00 23.20

29232A.D SCAN508.M Fri Feb 22 11:44:19 2002 Page 15

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