GCMS analysis report for sample AE01547, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB21\01547.D Vial: 3 ‘ Acq On : 21 Feb 2002 4:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 7 2,5-Cyclohexadiene-1,4-dion... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

13.38 0.07 ug/L 41156 Naphthalene-d8 13.20

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2,5-Cyclohexadiene-1,4-dione, 2,... 140 C6H404 000615-94-1 56 2 2,5-Cyclohexadiene-1,4-dione, 2,... 140 C6H404 000615-94-1 56 3 Uracil, 5-ethyl- $$ 2,4(1H,3H)-P... 140 C6H8N2O2 004212-49-1 50 4 2,5-Methano-2H-furo[3,2-b]pyran,... 140 C8H12O2 029946-84-7 9 Abundance Scan 886 (13.376 min): 01547.D (-) m/z 140.00 100.00% VO

5000

59 70 94 13.00 13.20 13.40 13.60 13.80 .............. I 0 I ‘ 1 ’1****1**AI* ■ 111 .-p • i ■ ■ ■ ■ i • ■ ■ ‘ i 1 1 • 4 I 1 1 | TI m/z 70.00 20.51% nz-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35122:2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- $$ p-... vo

5000 42 ■ i > ' 71 13.00 13.20 13.40 13.60 13.80 84 m/z 94.00 16.49% 53 94 112 01 ।1' ■' । T-p-T-r-TT-p-TT-r-p - -r-p-n-r-p-r I— niz- > :30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35123:2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- VO --------- 13 00 13.20 13.40 13.60 13.80 42 5000 m/z 59.10 16.37% 69

53 84 94 112 niz-> 01 I ' ‘ ' 1 1 30 40 50 60 70 TI8 80 -mp I 140 1-rT 90 100 110 120 130 Abundance #35153: Uracil, 5-ethyl- $$ 2,4(1 H,3H)-Pyrimidinedione, 5-... - r' p ' 1 ' i 1 VO 13.00 13.20 13.40 13.60 13.80 125 m/z 66.10 16.04% 82 5000

54 68 96 0 I 1 4 1 ■ i ■ ■ • ■ i ■ 1■■ i ■ ■■ 1 I ■ 1 ■ ■ i | 111 lpl t*ran । । In P । i i fl । i । p । 1—I miz—> 30 40 50 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

01547.D HP022102.M Mon Feb 25 10:55:25 2002 Page 9

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