GCMS analysis report for sample AE01510, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report • Data File : C:\MSDCHEM\l\5973N\02FEB21\01510.D Vial: 5 Acq On : 21 Feb 2002 2:17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 2,5-Cyclohexadiene-1,4-dion... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

13.38 0.05 ug/L 32628 Naphthalene-d8 13.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,5-Cyclohexadiene-1,4-dione, 2,... 140 C6H404 000615-94-1 72 2 4-Cyclopentene-1,3-dione, 4-meth... 140 C7H803 007180-62-3 64 3 Pyridine, 4-nitro-, 1-oxide (CAS... 140 C5H4N2O3 001124-33-0 50 4 2,5-Cyclohexadiene-1,4-dione, 2,... 140 C6H404 000615-94-1 40 Abundance Scan 886 (13.376 min): 01510.D (-) m/z 140.00 100.00% 140

5000 ................................................ 70 49 59 | 86 94 1300 13.20 13.40 13.60 13.80 Of • ■ i ■ ■ ‘ * i 1 ' 1 *'i ‘ 1 ■ ‘ i ' 1 । '• m agi 1........ m/z 70.00 15.55% miz-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35122:2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- $$ p-... 140

5000 42 ' 1 I ‘ ‘ 1 ‘ I ‘

71 13.00 13.20 13.40 13.60 13.80 84 m/z 94.10 14.67% 53 112 94 Ot ' 1 1 ' ' 1 1 T IUTt 1111 ■ 1 “ ' I ' — I 1 1 • 1 I T-r-p-r-n-p-r - miz-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35333:4-Cyciopentene-1,3-dione, 4-methoxy-5-methyl- 83 1-0 1 p ■ ■i■■■■i‘ 13.00 13.20 13.40 13.60 13.80 5000 m/z 66.00 8.95%

70 59 97 1 -H I I 4 | IT-mmptpt 111 125 — 01 * nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35067: Pyridine, 4-nitro-, 1-oxide (CAS) $$ p-Nitropyridi... 1-0 13.00 13.20 13.40 13.60 13.80 m/z59.10 8.80%

5000 39 110 45 51 63 N 94 124 . 84 | 0 •■i* m ' l I I ' 1 rr > ■ rpeh 1 i ■ • • • 1 ■ ’II - i > * - * i • 1 i ■ ■ ■ ■ i ■ m/z—> 30 40 50) 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

01510.D HP022102.M Mon Feb 25 10:55:10 2002 Page 10

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