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GCMS blank analysis results for sample AE03508, March 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS blank analysis results for volatile organic compounds with detection limits below MDL.

NYC-WTC_000037616–000037634

Folder label: “GCMS X 2/19/02 A 3/8/02

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NYC 9/11 Public Portal Document

Library Search Compound Report * Data File : C:\MSDCHEM\l\5973N\02MAR08\0219B.D Vial: 1 Acq On : 8 Mar 2002 10:39 am Operator: Sample : lab blank 2/19 Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 2,5-Cyclohexadiene-1,4-dion... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 13.38 0.06 ug/L 40306 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2,5-Cyclohexadiene-l,4-dione, 2,... 140 C6H404 000615-94-1 72 2 l-Oxetan-2-one, 4,4-diethyl-3-me... 140 C8H12O2 000000-00-0 56 3 Pyridine, 4-nitro-, 1-oxide (CAS... 140 C5H4N2O3 001124-33-0 56 4 3H-Pyrazol-3-one, 2,4-dihydro-2,... 140 C7H12N20 003201-25-0 42 Abundance Scan 886 (13.376 min): 0219B.D (-) m/z 140.00 100.00% 140

5000 ................ . 44 70 84 96 13.00 13.20 13.40 13.60 13.80

miz-> 01 ■' । ■ •' ■ । ■1 ■ ‘ i • ‘ 30 40 50 60 70 80 4 TI—wI—1-rtt1rr | I ‘ 1 ' 1 I 90 100 110 120 130 140 m/z 96.10 11.95% Abundance #35122: 2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- $$ p-... 140

1 ‘ -------- 5000 42 TIII 71 13.00 13.20 13.40 13.60 13.80 m/z 70.10 11.74% 53 84 112 — 94 Of ■ • i ■ ■ • * I TT-p-r-n-p-r TIt — - m/z—> 30 40 50 60 70 80 90I 100 110 120 130 140 Abundance #35765:1-Oxetan-2-one, 4,4-diethyl-3-methylene- 79 1-0 39 67 ■ i ■ ■ 13.00 13.20 13.40 13.60 13.80 125 5000 53 111 m/z 94.10 11.74% 97

Of ■ ‘ i ■ ■ ■ ■ i ' ■ 1 ‘ t ■ ■ ■ ■ i • 1 I r-p miz-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35067: Pyridine, 4-nitro-, 1-oxide (CAS) $$ p-Nitropyridi... / —I11PTT • i ■ ■ ■ ■ । 1-0 13.00 13.20 13.40 13.60 13.80 m/z 83.90 10.24%

5000 39 110 51 45 63 124 84 94 O *•i* r-p-rTT-p-r-TT-p -—■ i ■ 1 ■‘ i ‘ ■ TTT m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

0219B.D HP022102.M Fri Mar 15 10:08:44 2002 Page 13

NYC-WTC_000037631

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NYC-WTC_000037631Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.995

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