Laboratory report showing GCMS blank analysis results for volatile organic compounds with detection limits below MDL.
NYC-WTC_000037616–000037634Folder label: “GCMS X 2/19/02 A 3/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report « Data File : C:\MSDCHEM\l\5973N\02MAR08\0219B.D Vial: 1 Acq On : 8 Mar 2002 10:39 am Operator: Sample : lab blank 2/19 Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.10 ug/L 85392 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 3 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 4 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2: 000000-00-0 46 Abundance Scan 1675 (22.283 min): 0219B.D (-) m/z 192.00 100.00% 192
5000
96 146 160 • * i ■ • • । • .. RR 82। 22.00 22.20 22.40 22.60 44 00 । 120 | o prup ...plirp-nl-illr.pl -q-rr WIuOppo mH m/z 191.00 20.68% mfe-> 2030405060 70 8090 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588: 4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192
5000 108
146 175 m/z ■ ■ i ‘ ■ i ‘ ‘ L 22.00 22.20 22.40 2260 95.90 16.28%
m/z—> 0 -rrTTpTT-ryTTTTpTTTTTTTTTTTTTpT-rrp^ I''“I‘ 'I''''I'' ‘I I I ' ' ' 'I ' h..... T 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192 ' ‘ I ‘ ‘ ‘ ‘ I ‘ ‘ ’11/1/111/11 22.00 22.20 22.40 22.60 5000 82 m/z 193.00 15.26% 54 110
m/z—> 0 30 mm T-rp-rT-rp-r m mppnpmpmtmnpt 1 94 160 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 IM 200 ‘trrj-r
Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene -PP ■ ■ i ■ ■ ■ 1 i 1 192 22.00 22.20 22.40 22.60 m/z 146.10 13.93% 5000
mfz~> 96 88 1 165 139 152 0 176 0 "ULOTIUTI n 11P । TIUTTTT;, p 11,11. i TTTghgom , 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 u T T 22.00 22.20 22.40 22 60 III
0219B.D HP022102.M Fri Mar 15 10:08:44 2002 Page 14
NYC-WTC_000037632
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NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037760
Laboratory report documenting GCMS analysis of a method blank for sample AE03615 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037740
Laboratory report documenting GCMS analysis of a method blank for sample AE03614 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051512
Laboratory report showing GCMS blank analysis results for sample AE00555 conducted between January 29 and February 1, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010843
Laboratory report documenting a blank run for gas chromatography-mass spectrometry analysis of sample AE02713.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052029
Laboratory report showing GCMS blank analysis of sample AE00830 with compounds below detection limits.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009918
Calibration data for GCMS analysis including response factors for various organic compounds recorded on February 21, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006105
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03246 conducted on March 15, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050189
Blank analysis report for GCMS testing of sample AD31647 confirming no contamination above detection limits.
1 shared non-person entities · 1 shared topics · similarity 0.994
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NYC-WTC_000037604
Department of Environmental Protection site log sheet for the World Trade Center area covering February and March 2002.
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NYC-WTC_000037605
Record of water sample extraction parameters including drip rates, volumes, and pH measurements from February to March 2002.
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NYC-WTC_000037611
Reference standard analysis data verifying instrument performance for detecting volatile organic compounds in water samples.
Filed in the same folder
NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
Filed in the same folder
NYC-WTC_000037655
Laboratory report listing concentrations of volatile organic compounds in sample AE03509 analyzed on March 19, 2002.
Filed in the same folder