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GCMS blank analysis results for sample AE03508, March 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS blank analysis results for volatile organic compounds with detection limits below MDL.

NYC-WTC_000037616–000037634

Folder label: “GCMS X 2/19/02 A 3/8/02

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NYC 9/11 Public Portal Document

Library Search Compound Report * Data File : C:\MSDCHEM\l\5973N\02MAR08\0219B.D Vial: 1 Acq On : 8 Mar 2002 10:39 am Operator: Sample : lab blank 2/19 Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 1,2-Benzenedicarboxylic aci... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.09 ug/L 65039 Chrysene-dl2 30.49 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,2-Benzenedicarboxylic acid, 3-... 211 C8H5NO6 000603-11-2 83 2 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 027554-26-3 78 3 1,2-Benzenedicarboxylic acid, bi... 390 C24H3804 000117-81-7 78 4 Phthalic acid, diisooctyl ester ... 390 C24H3804 001330-91-2 78 Abundance Scan 2455 (31.088 min): 0219B.D (-) m/z 149.00 100.00% 149

5000 43

0- ■ — • • I । — • 57 70 | 83 113 । 167

240 _ s— m/z 30.80 31.00 31.20 31.40 57.10 37.55% 80 100 120 140 160 180 200 220 — miz-> 40 60 240 Abundance i#131213:1,2-Benzenedicarboxylic acid, 3-nitro- (CAS) $$ 3... 149

5000 30.80 31.00 31.20 31.40 167 71 m/z 167.00 32.11%

miz-> 0- 4 I • ‘ 40 • I 1 60 1 80 83

100 113

120 132 ill. 140 1 1 ' ■ ' i 1 1 ■ • i ■ ■ ■ 1 i ■ ■ ■ ■ I ■ ■ ■ ■ i ' • 160 180 200 220 240 Abundance #326921:1,2-Benzenedicarboxylic acid, diisooctyl ester (C... 149

130.80 31.00 31.20 31.40 5000 m/z 43.10 25.09% 57 167 71 — — ■ 83 — —% I1'113 L i ■ ■ 0- ■ ' 1 1 ‘ ‘ I ‘ 1 ' ' I ‘ ' I ‘ ‘ I ■ ■ ' ■ I ‘ ■ miz—> 40 60 80 100 120 140 160 180 200 220 240 Abundance #326907:1,2-Benzenedicarboxylicacid, bis(2-ethylhexy!) e... 149 130.80 31.00 31 ■20' 31.40 ' m/z 55.10 20.12% 5000 57 167 71

miz-> 0 —42 83 97 113 40 60 I H ■ — I'. r IP 80 100 120 — 140 160 1 1 • i ■ • ■ • i • ■ ■ ' i ' ■ ■ ■ i ■ ' 180 200 220 240 T T ICT 30.80 31.00 31.20 31.40

0219B.D HP022102.M Fri Mar 15 10:08:45 2002 Page 15

NYC-WTC_000037633

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NYC-WTC_000037633Source: NYC Law Department, mirrored locally

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