GCMS analysis results for sample AE01507, Mar 2002

NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C:\MSDCHEM\1\5973N\02FEB21\01506.D Vial: 3 Acq On : 21 Feb 2002 12:31 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 l-Oxetan-2-one, 4,4-diethyl... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

13.39 0.08 ug/L 48900 Naphthalene-d8 13.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l l-Oxetan-2-one, 4,4-diethyl-3-me... 140 C8H12O2 000000-00-0 64 2 2,5-Cyclohexadiene-1,4-dione, 2,... 140 C6H404 000615-94-1 56 3 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 50 4 3H-Pyrazol-3-one, 2,4-dihydro-2 ,... 140 C7H12N20 003201-25-0 9 Abundance Scan 887 (13.387 min): 01506.D (-) m/z 140.00 100.00% VO

5000

iz—> 43 | 0 1’*’’I**AIS ■ 30 40 50 60 70 1.1 ■■■ 70 80 —1 90 100 110 120 130 140 1300 13.20 13.40 13.60 13.80 m/z 93.90 15.87% Abundance #35765:1-Oxetan-2-one, 4,4-diethyl-3-methylene- 79 VO 39 67 125 - 5000 53 111 97 1300 13,20 13.40 13.60 13.80 m/z 69.90 13.02%

miz—> 0 --- 30 40 50 60 70 80 90 100 110 ■ Ji.. 120 J.i.. || 130 140 TII Abundance #35122:2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- $$ p-... VO ....... \ ■ i ■ ■ ■ ‘ i ‘ ■ i ■ ■ ■ ■ i ■ 1 13.00 13.20 13.40 13.60 13.80 5000 42 m/z 96.10 12.50% 71 53 49.. 112.... m/z—> 6I1111I 30 40 • ■ i1 ■1 • i ■ ■ 50 60 70 80 90 100 110 120 130 -T 140 Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 1**11** • ■ i ■ • ■ ■ i ■ 1 VO 13.00 13.20 13.40 13.60 13.80 m/z 66.00 9.52% 5000

44 71 123 . 86 96 112 - i I mfe-> oV 30 .40+-pp50 . 60. 70 80 90 100 110 120 130 140 TII ■ l ■ • ■ > I ■ • » • 1 > i 13.00 13.20 13.40 13.60 13.80

01506.D HP022102.M Mon Feb 25 10:54:44 2002 Page 8

NYC-WTC_000009957