GCMS analysis results for sample AE01507, Mar 2002

NYC 9/11 Public Portal Document

Library Search Compound Report • Data File : C: \MSDCHEM\1\5973N\02FEB21\01506.D Vial: 3 Acq On : 21 Feb 2002 12:31 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 7 Hexadecane (CAS) $$ n-Hexad... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 19.92 0.20 ug/L 134936 Acenaphthene-dl0 18.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexadecane (CAS) $$ n-Hexadecane... 226 C16H34 000544-76-3 86 2 Heptadecane $$ n-Heptadecane $$ ... 240 C17H36 000629-78-7 86 3 Octane, 2,4,6-trimethyl- 156 C11H24 062016-37-9 80 4 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 80 Abundance Scan 1466 (19.923 min): 01506.D (-) m/ z 57.10 100.00% 57

71 43 5000 85

A--—PPA 99 143 19.60 19.80 20.00 20.20 0- 1113/127. * I ‘ 4 1 • l 1 ‘ ‘ • I 4,4814**1** ■ ‘ 164 ‘ ‘ । ‘ ■ i 1 ■ ■ ■ । • • ■ • । • m/z 71.10 65.45% mz—> 40 60 80 100 120 160 . 180 140 200 220 240 Abundance #154906: Hexadecane (CAS) $$ n-Hexadecane $$ Cetane $$ n-C... 43 57 71 / 5000 i • ■ ' 1 i 85 19.60 19.80 20.00 20.20 m/z 43.10 59.03% , 99 113 127 141 155 0-■ * i ‘ • 1 i » I, , t [I, , " l./"/ miz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #174546: Heptadecane $$ n-Heptadecane $$ Normal-heptadecane 57 71 1A1uii AM/ —PAP, 85 19.60 19.80 20.00 20.20 5000' m/ z 85.10 46.45% 99 il 113 127 141 196 240 0-■ • I 1 1 1 ‘ I 1 ■ • • i । ■ 11i1'।'।1'11i'111r11'1 r111'i’1 r■i 11 * ‘i ■ 40 60 80 100 120 140 160 180 200 220 240 Abundance #56276: Octane, 2,4,6-trimethyl- ----- 57 19.60 19.80 20.00 20.20TTT m/z 41.10 26.26% 5000 71 85 99

mz—> 0—m—TT 40 60 80 1 127 ■ I ■ 1 ' ■ i • 100 120 • i ■ ■ • ■ i • • ■ ■ i ■ ‘ 140 160 180 ■ i ‘ 200 ‘ ‘ i ■ • ‘ ■ i ■ 1 220 240 -AALAA 19.60 19.80 20.00 20.20 —

01506.D HP022102.M Mon Feb 25 10:54:44 2002 Page 9

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