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GCMS analysis results for sample AE00838, Feb 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE00838 including surrogate recovery and unknown compounds.

NYC-WTC_000052187–000052204

Folder label: “GCMS X 1/11/02 A 1/31/02

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Scanned page image, NYC-WTC_000052196
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00831.D Vial: 4 Acq On : 31 Jan 2002 1:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Hexadecane Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T. 19.92 0.41 ug/L 278644 Acenaphthene-dl0 18 34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecane 226 C16H34 000544-76-3 94 2 Hexadecane (CAS) $$ n-Hexadecane... 226 C16H34 000544-76-3 93 3 Hexadecane 226 C16H34 000544-76-3 93 4 Hexadecane (CAS) $$ n-Hexadecane... 226 C16H34 000544-76-3 93 Abundance Scan 1449 (19.917 min): 00831 .D (-) m/z 57.10 100.00% 57

43 71 5000 85

99 19.60 19.80 20.00 20.20 „ I 112 127 140 155 226 0 ml TTTTTTTITT TTTTTTTTTT m/ z 71.10 61 01% m/z-> 30 40 50 60 70 80 90 100110120130140150160170180190200210220230 Abundance #154905: Hexadecane 57 43

5000 71 W VAT , I I IT TY 19.60 19.80 20.00 20.20 85 m/z43.10 56.75%

m/z-> 0 mm 99 113 127 HTTTTTTTTTTTTWTTTTTTT " 11"11" " i 30 40 50 60 70 80 90 100110120130140150160170180190200210220230 226 I" 1' i

Abundance #154903: Hexadecane (CAS) $$ n-Hexadecane $$ Cetane $$ n-C... 57 71 19.60 19.80 20.00 20.20 85 m/z85.10 43.08% 5000

4 99

m/z-> 0 mipylm 113 141 155 169 182 TTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT 226 I'....... "I 30 40 50 60 70 80 90 100110120130140150160170180190200210220230 -====24== Abundance #154904: Hexadecane 57 19.60 19.80 20.00 20.20 m/ z 41.10 23.23% 71 5000 85

99 113 127 141 155 169 183 226 - ITTi | I Pl I | I I ! I1! I I I I | l'l ! I |TTf'l | rerfnm’ I I l'| I I ( I | I'l I I TTHTT 0- F"11" " I /z-> 30 40 50 60 70 80 90 100110120130140150160170180190200210220230 19.60 19.80 20.00’ 20.20

00831.D SCAN508.M Fri Feb 01 09:18:43 2002 Page 8

NYC-WTC_000052196

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NYC-WTC_000052196Source: NYC Law Department, mirrored locally

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