GCMS surrogate recovery results, sample AE07115, April 15, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohlk Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 3 Hexadecane (CAS) $$ n-Hexad... Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T.

25.07 5.80 ug/L 890233 Phenanthrene-dl0 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecane (CAS) $$ n-Hexadecane... 226 C16H34 000544-76-3 91 2 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 90 3 Eicosane (CAS) $$ n-Eicosane 282 C20H42 000112-95-8 90 4 Hexadecane 226 C16H34 000544-76-3 .90 Abundance Scan 3743 (25.072 min); 7115.D (-) m/ z 57.10 100.00% 57

5000 85

m/z-> 0 jLLLux 205 n f. . .1 I I f. ■ P ■! r| I I I 260- 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 *Kbundance #154903: Hexadecane (CAS) $$ n-Hexadecane $$ Cetane S$ n-C... m/z 24.80 25.00 25.20 25.40 71.10 58.23%

57

5000 85 24.80 25.00 25.20 25.40 m/z 43.10 46.16% 4' , A j J 141 169' 197 226 0 tJ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #245745: Heneicosane SS n-Heneicosane 57

24.80 25.00 25.20 25.40 85 m/z 85.15 39.22% 5000

A 41 IIS

Tl/Z-> 0 15 ,! , "I 'r 4^J J jA ^69 . 197 225 253 . I-T, I n .. I > > 111, r I. I* .. 11. .-I,, r, 111.1.. I 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 296 ,-r^

Abundance #228982; Eicosane (CAS) $S n-Eicosane 5(7 24.80 25.00 25.20 25.40 m/z 41.10 19.48%

5000 85

m/z-> 0 JU 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 24.80 25.00 25.20 25.40

7115.D 5080402BB.M Mon Apr 15 18:16:25 2002 Page 6

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