Laboratory report showing GCMS blank analysis results for volatile organic compounds with detection limits below MDL.
NYC-WTC_000037616–000037634Folder label: “GCMS X 2/19/02 A 3/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
• Data File : C:\MSDCHEM\l\5973N\02MAR08\0219B.D Vial: 1 Acq On : 8 Mar 2002 10:39 am Operator: Sample : lab blank 2/19 Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Cyclopentasiloxane, decamet... Concentration Rank 13
R.T. EstConc Area Relative to ISTD R.T.
12.54 0.04 ug/L 30705 Naphthalene-d8 13.20
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 N-Methyladrenaline, tri-TMS 413 C19H39NO3Si3 000000-00-0 38 3 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 33 4 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 32 Abundance Scan 812 (12.540 min): 0219B.D (-) m/z 73.00 100.00% 73
5000 267 355 ---
-+ ■ ■ i ■ ■ ' 1 i ‘ 44 12.20 12.40 12.60 12.80 0- ■ iI1 “i ‘ i" ------------------------------ I'' " I m/z 266.90 45.26% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313065: Cyclopentasiloxane, decamethyl- 73
5000 267 ' 1 1 । i i । i i 1’—— 12,20 12.40 12.60 12.80 355 m/z 355.00 32.85%
m/z—> 45 | । 0- Th*mmppmpago 40 60 193 223 4 —323339.4— 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #339188: N-Methyladrenaline, tri-TMS 58 75 T-TT-rnr-r-T-f-rT ■ I ' ‘ ‘ ‘ I ' ‘ ‘ ‘ I 12.20 12.40 12.60 12.80 50001 355 m/z 356.00 12.77%
207 If; 1 0- i 162415 . ............267282 P 200323 1 ’ * 1 1 1 * 1 j * * * 118 1 1 1 | » i » : j i i j i । « Irr m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313068: Cyclopentasiloxane, decamethyl- TETX—n—/O/m i ■ ■ ■ • i ■ ■ • ■ i 73 12.20 12.40 12.60 12.80 m/z74.10 8.25% 355 267 5000
251 । 323339 , 11, 0 1—011—munuu*OEOTTI 191207 Pmm F’T T’EnnImT ‘ i • ■ • ‘ i • ■ • ■ i m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 12,20 12,40 12.60 12.80
0219B.D HP022102.M Fri Mar 15 10:08:44 2002 Page 12
NYC-WTC_000037630
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NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037760
Laboratory report documenting GCMS analysis of a method blank for sample AE03615 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037740
Laboratory report documenting GCMS analysis of a method blank for sample AE03614 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051512
Laboratory report showing GCMS blank analysis results for sample AE00555 conducted between January 29 and February 1, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010843
Laboratory report documenting a blank run for gas chromatography-mass spectrometry analysis of sample AE02713.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052029
Laboratory report showing GCMS blank analysis of sample AE00830 with compounds below detection limits.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009918
Calibration data for GCMS analysis including response factors for various organic compounds recorded on February 21, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006105
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03246 conducted on March 15, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050189
Blank analysis report for GCMS testing of sample AD31647 confirming no contamination above detection limits.
1 shared non-person entities · 1 shared topics · similarity 0.994
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NYC-WTC_000037604
Department of Environmental Protection site log sheet for the World Trade Center area covering February and March 2002.
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NYC-WTC_000037605
Record of water sample extraction parameters including drip rates, volumes, and pH measurements from February to March 2002.
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NYC-WTC_000037611
Reference standard analysis data verifying instrument performance for detecting volatile organic compounds in water samples.
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NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
Filed in the same folder
NYC-WTC_000037655
Laboratory report listing concentrations of volatile organic compounds in sample AE03509 analyzed on March 19, 2002.
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