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GCMS blank analysis results for sample AE03508, March 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS blank analysis results for volatile organic compounds with detection limits below MDL.

NYC-WTC_000037616–000037634

Folder label: “GCMS X 2/19/02 A 3/8/02

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NYC 9/11 Public Portal Document

Library Search Compound Report * Data File : C:\MSDCHEM\l\5973N\02MAR08\0219B.D Vial: 1 Acq On : 8 Mar 2002 10:39 am Operator: Sample : lab blank 2/19 Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Hexane, 2,2,5-trimethyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 9.94 0.13 ug/L 63134 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexane, 2,2,5-trimethyl- 128 C9H20 003522-94-9 9 2 Hexane, 2,2-dimethyl- 114 C8H18 000590-73-8 9 3 Pentane, 3-ethyl-2,2-dimethyl- 128 C9H20 016747-32-3 9 4 Pentane, 3-ethyl-2,2-dimethyl- 128 C9H20 016747-32-3 9 Abundance Scan 582 (9.944 min): 0219B.D (-) m/z 57.10 100.00%’ 57

5000 41 49 71 —A 9.60 UAAA 9.80 10.00 10.20

miz-> O' “(““12’31’22/157 mm lmmmmmmmmmmmmm 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 115120 m/z 56.10 42.49% Abundance #25224: Hexane, 2,2,5-trimethyl- 57 — 5000 rT Trrr T 9.60 9.80 10.00 10.20 41 71 m/z 59.10 26.19% 27 113 mppmptmmmmmTTT 01 mpdp mH — miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #15659: Hexane, 2,2-dimethyl- 57 M 9.60 9.80 AA 10.00 10.20 5000 m/z 41.10 25.34% 41 29 O mHm ■ i “"i" “ trp-rrrpT-r. ,........70..................... 99.................. Illi,III III “’CU13T1" 1111111 "—"010311117 , "IEE11T miz—> 20 25 30 35 40 45 50 55 30 35 70 75 80 85 90 95 100105110115120 Abundance #25243: Pentane, 3-ethyl-2,2-dimethyl- 57 9.60 9.80 10.00 10.20 1 ‘ m/z 43.10 22.70% 5000 41

miz-> 0 27 l.. +mm 71 T,’—nuIn3"u11 AA 84......................................... ,||—O—1—E10—E1U"EOE9 20 25 30 35 40 45 5C 55 60 65 70 75 80 85 90 95 100105110115120 —E1IEEE“——EI——II1"IIT uhAAAN 9.60 9.80 10.00 10.20 • ■ i 1

0219B.D HP022102.M Fri Mar 15 10:08:44 2002 Page 11

NYC-WTC_000037629

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NYC-WTC_000037629Source: NYC Law Department, mirrored locally

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