DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB26\02086.D Vial: 3 Acq On : 26 Feb 2002 4:27 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 26, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 8 2,5-Cyclohexadiene-l,4-dion... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

13.38 0.05 ug/L 35063 Naphthalene-d8 13.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,5-Cyclohexadiene-1,4-dione, 2,... 140 C6H404 000615-94-1 83 2 2,5-Cyclohexadiene-l,4-dione, 2,... 140 C6H404 000615-94-1 74 3 2-Hydroxy-5-nitropyridine $$ 5-N... 140 C5H4N2O3 005418-51-9 40 4 3H-Pyrazol-3-one, 2,4-dihydro-2,... 140 C7H12N20 003201-25-0 9 Abundance Scan 886 (13.376 min): 02086.D (-) m/z 140.10 100.00% 140

5000

44 66 94 112 13.00 13.20 13.40 13.60 13.80 0+ ----- ------------- I 1II m/z 66.00 11.48% miz-> :30 40 50 60 70 80 90 100 110 120 130 140 f Abundance #35123:2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- 14.0

42 5000 69 13,00 13.20 13.40 13.60 13.80 84 m/ z 44.00 11.33% 53 94 112

hMond Ot— T-r-i-r - TTd m/z- > 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35122: 2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- $$ p-... 140

13,00 13.20 13,40 13,60 13.80 5000 m/z 141.10 11.18% 42 71 53 84 112 94 01 i ‘ ■ ■ ■ i 1 ■ i 1 ' ' ' i ' ' 11 ' ' ' I ' — i 1 ' ■ 1 i ■ 1 । 1 < 1 > i 1 1 - m/z- > 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35063:2-Hydroxy-5-nitropyridine $$ 5-Nitro-2-hydroxypyri... 1 1 I 1 ' ' 1 1 1 VO 13.00 13.20 13.40 13.60 13.80 m/z 94.00 10.85%

5000 66

80 110 49 — 124 | 0 i ■ ■ ■ ■ । ■ ■ ■ ■’i ■ ■ ■ ■ i > -1 1 1 1 TTI m/z-> 30 40 50 60I 70 80 90 100 110 120 130 140 13.00 13.20 13.40 13.60 13.80

02086.D HP022102.M Wed Feb 27 08:35:02 2002 Page 10

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