GCMS analysis report for sample AE01510, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report / Data File : C:\MSDCHEM\l\5973N\02FEB21\01510.D Vial: 5 Acq On : 21 Feb 2002 2:17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 2-Propanol, 1-(2-methoxypro... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

9.88 0.17 ug/L 77760 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 74 2 Butane, 2-methoxy- (CAS) $$ Meth... 88 C5H120 006795-87-5 9 3 Butane, 2-methoxy- $$ Ether, sec... 88 C5H120 006795-87-5 9 4 3-Hexanol (CAS) $$ Hexan-3-ol $$... 102 C6H140 000623-37-0 9 Abundance Scan 576 (9.876 min): 01510.0 (-) m/z 59.10 100.00% 59

5000 .. .....................................

45 73 104 9.60 9.80 10.00 10.20 0-1*12/n/n————/m—nOTTntt30*2m2tpuu 1 84 ’!—t—tu—1 u——’3—31tt m/z 73.00 15.19% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #43942:2-Propanol, 1-(2-methoxypropoxy)-$$ 1-(2-Methoxyp... 59

5000 _AA9.60 9.80 10.00 10.20 m/z 45.10 15.12% 31 45 7 . 194. 130 ........... lasal,...... lY ■. ’I***41***

MA 0- ’1*’’I’’*’I***’I’’I** m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4937: Butane, 2-methoxy- (CAS) $$ Methyl sec-butyl ether... 50 • ‘ I •» 9.60 9.80 10.00 10.20 50001 m/z 41.10 12.04% 15 27 73 45

miz-> 0- mmt 10 20 30 40 - -33— 50 60 ■ i | 88 ‘1 ■ ■ i ■ ■ ■11 ■ •1 ■ i 1 ' ■ ‘ i ■ ■ ■111 • 11 I' 1 70 80 90 100 110 120 130 Abundance #4938: Butane, 2-methoxy- $$ Ether, sec-butyl methyl $$ se... 59 9.60 9.80 10.00 10.20 m/z 42.10 11.46% 5000

15 27 73

mfz~> +B3ll 0 T-r-p-rh-r-p- 10 20 | 88 70 80 90 100 110 120 130 30 40 50 60 ■ i ■ ■■■i1■i■■ ■ ■ i ■ ■ ■ ■ i1 ■ ■ ■ i ■1 ■ ■i'■ ---PPPP 9.60 9.80 10.00 10.20

01510.D HP022102.M Mon Feb 25 10:55:10 2002 Page 9

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