GCMS DFTPP calibration report, Feb 5 2002

Machine-extracted title · confidence 95%

Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

* Data File : C:\MSDCHEM\1\5973N\02FEB05\29232A.D Vial: 4 Acq On 5 Feb 2002 1:13 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 8 2-Propanol, 1-(2-methoxypro... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

9.85 0.06 ug/L 48769 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 83 2 PROPYLENE GLYCOL TRIMER 1 174 C9H18O3 000000-00-0 43 3 Butane, 2-methoxy- $$ Ether, sec... 88 C5H120 006795-87-5 43 4 Butane, 2-methoxy- (CAS) $$ Meth... 88 C5H120 006795-87-5 43 Abundance Scan 567 (9,847 min): 29232A.D (-) m/ z 59.10 100.00% 59

5000

— 45 73 104 AN 9.60 9.80 10.00 10.20 0 ■ । I 84 । i ■ । । • • ■ > । I > i • ■ ■ > i ■ ■ ■ ■ i > ■ m/z 45.10 14.33% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #43942:2-Propanol, 1 -(2-methoxypropoxy)- $$ 1-(2-Methoxyp... 59

5000 9.60 9.80 10.00 10.20 m/2 73.10 12.55% 31 45 0 .......... |........ I,, ' ■ i1".1......... .. 73 194 ' i ' ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ' ' ■ ' i ■ ■ ' 1 i ■ ■ ■ ■ i ' ■ 130 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #78532: PROPYLENE GLYCOLTRIMER 1 59 AN, A । ,,,,,,, , 9,60 9,80 10.00 10.20 5000 41 m/z 41.10 9.22% 103

73 87 117 130 0- — - m/z-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 #4938: Butane, 2-methoxy- $$ Ether, sec-butyl methyl $$ se... 130 4.., 59 9.60 9.80 10.00 10.20 m/z 43.10 8.80%

5000 A

15 27 45 73 0 1 ' I 1 1 1 1 I 1 —33— | 88 1 1 1 ' 1 ' I ■ • ■ ' i ' ' • ■ i ' ■ ' ■ i ‘ ' 1 ■ i ' ' ' 1 i ' ' mlz~> 10 20 30 40 50 60 70 80 90 100 110 120 130 9.60 9.80 10.00 10.20

29232A.D SCAN508.M Fri Feb 22 11:44:19 2002 Page 10

NYC-WTC_000004889

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