GCMS analysis results for sample AE03252, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03252 conducted on March 15, 2002.

NYC-WTC_000006226–000006245

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document WIL—/—

Data File : C:\MSDCHEM\1\5973N\02MAR01\03252.D Vial: 7 • Acq On : 1 Mar 2002 8:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Cyclopentasiloxane, decamet... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 12.54 0.12 ug/L 79551 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 43 3 12.BETA.-OCTAHYDROINDOLO [2,3-A]Q... 356 C21H28N2O3 065634-80-2 38 4 3,4-DIHYDROXYMANDELIC ACID-TETRATMS 472 C20H4005Si4 000000-00-0 38 Abundance Scan 812 (12.541 min): 03252.D (-) m/ z 73.10 100.00% 73

267 5000 355

..................../ ........................ 45 162 193 12.20 12.40 12.60 12.80 mj..— ■ ■ ।'' ■ ■ ।11 0 111I ■■■।■1■।1 ■ ■11' ■' ■ ।1 ‘1' । ■11' I' ■ ■11 ■1 ■ ■ । ■ ■111 ■ ■ ■ ■ ।1 F" m/z 266.90 53.46% /z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

. ................................................................................................... \ ;■.....................................................................................................

5000 267 12.20 12.40 12.60 12.80 355 m/z 355.00 47.13% 45 193 223 251 J 1 | 0 TLTTTETTTLTTTTTTTTTTTTTTTTTTTTTTITTTTIWWTTTTLTTTDT ■ ■ i ■ ■ । ■ i ■ ■ ■ ■ 1 ‘ 323339 j ■ 11 ■ ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 12.20 12.40 12.60 12.80 267 m/z 356.00 19.11% 5000

, , 191207 323339 251 | TIUTTTITTTTTTT 0 ' I''11 'l11' ’ 1111' 1111' 1'11' I'11111 " 1111Y' I i 1 1 I I I ' ' I I l l‘ I I l ] >. I

miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #303262:12.BETA.-OCTAHYDROINDOLO[2,3-A]QUINOLIZINE$$ 1,1... 267 12.20 12.40 12.60 12.80 m/z 267.90 12.80%

5000 356 169 0 11’1a1111na1’111j’oaw1’111111o*12111*1/4**///1GGGI ■ ■ । ■ ■ ■ ■ । • ■ ■ ■ । > ■ ■ ■ । ■ T ' 1 i ■ ■ ■ ■ i 1 1 I 1 1 1 । I ' 1 TTT n/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 12.20 12.40 12.60 12.80

I3252.D HP022102.M Mon Mar 04 12:33:54 2002 Page 7

NYC-WTC_000006236

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NYC-WTC_000006236Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE03248, March 2002 · Box DEP Box 12

NYC-WTC_000006146

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03248 conducted on March 15, 2002.

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