Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
NYC-WTC_000050481–000050499Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document **r***** -*£**
Data File : C:\MSDCHEM\1\5973N\02JAN24\00167.D Vial: 4 . Acq On : 24 Jan 2002 2:09 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1. . .\SCAN5 08. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 4-METHOXY-.BETA.-METHYLCINN. .. Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T. 22.28 0.16 ug/L 127342 Phenanthrene- dl 0 22.65
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 64 2 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 59 3 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N60 000945-24-4 59 4 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 Abundance Scan 1656 (22.280 min): 00167. D (-) m/z 192.10 100.00% 192
5000
96 146 160 70 82 n/z-> 42 Y p—o———ummpmap—H—HD—mT *Pmpp*ango , l 118 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 I 22.00 22.20 22.40 22.60 m/z 146.10 15.70% Abundance #102588:4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192
108 .AS...... M.7 5000 22.00 22.20 22.40 22.60 146 175 m/z96.10 14.51%
" i“ “ i " ■ ■ r ■" i ‘ " i' ■ " i‘' “ i‘'' • i" i " “ i ‘" i “ '' i ‘' ' i ■ ■ ■ ■ i ■■ ■‘ i ■ 'I '!'■■■ I1 TI’1 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192 **4’**’I**}’’’I’S 22.00 22.20 22.40 22.60 5000 m/z 191.00 13.87%
96 164 1 138 I.... ........ IL 1 ‘‘I 111 ‘“'I'“'I11 ‘ miz-> 30 40 50 60 70 80 100 110 120 130 140 150 160 170 180 190 200 Abundance #102010:2,4-Diamino-6-(hydroxymethyl)pteridine 192 22.00 22.20 22.40 22.60 163 m/z 193.00 13.09%
5000
66 146 175
/z-> 34 T’nt 11 ‘1 ‘ I ‘1 " I 121 1′34311..»11, >. I. I.. I. J.. II . I 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 135 i" “ i ‘ lII...... I * ’ ‘ I‘* 22.00 22.20 22.40 22.60
>0167.D SCAN508.M Fri Jan 25 10:25:48 2002 Page 12
NYC-WTC_000050496
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NYC-WTC_000050596
Laboratory report listing unknown compounds and surrogate recovery for sample AE00250 analyzed on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050519
Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050539
Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050735
Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050683
Laboratory report listing unknown compounds and surrogate recovery for sample AE00166 analyzed on February 13, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050645
Laboratory report listing unknown compounds and surrogate recovery for sample AE00110 analyzed on February 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051877
GCMS analysis log for sample AE00701 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000050432
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050433
Fragmented page containing a document identifier and instructions regarding liquid-liquid extractor drip rates from January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050435
Gas chromatography-mass spectrometry calibration analysis of sample AE00167 detecting multiple organic compounds including nitrosamines and dichlorobenzenes.
Filed in the same folder
NYC-WTC_000050439
Laboratory report listing concentrations of volatile organic compounds in sample AE00167 analyzed on January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050444
Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.
Filed in the same folder