Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
NYC-WTC_000050481–000050499Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document uJL aL y ocaiti Lopounu Kepo L
Data File : C: \MSDCHEM\1\5973N\02JAN24\00167.D Vial: 4 • Acq On : 24 Jan 2002 2:09 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2-Propanol, 1-(2-methoxypro. . . Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 9.86 0.08 ug/L 39936 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 64 2 Butane, 1-ethoxy- (CAS) $$ Ethyl... 102 C6H140 000628-81-9 9 3 Butanoic acid, 2-hydroxy- $$ But... 104 C4H803 000565-70-8 5 4 2-METHYL-3,3-D2 -AZIRIDINE 59 C3H5D2N 030691-55-5 4 Abundance Scan 568 (9.858 min): 00167.D (-) m/z 59.10 100.00% 59
5000
43 73 TT0aguu)2*T2mBTTTT104 m/z N 1 ‘ I ' ' ‘ ‘ I ‘ 9.60 9.80 10.00 10.20 43.10 12.25% ‘ ' I ■ NA > i ■ ■ ■ ■ i ■ * • • i ■ * । • • • * i ■ /z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #43942:2-Propanol, 1-(2-methoxypropoxy)-$$ 1-(2-Methoxyp... 59 MN 5000 -r ' I ' ■ ' ‘ T IUi8 TTT 9.60 9.80 10.00 10.20 m/z 41.10 9.99% 31 45 . I........ 1......... ’I1".......... I1!.. 73............. 104 .......... 130 ‘ I 1 ‘ * 1 ' ‘ 1 ’ I ‘ ‘ * I ‘ 1 1 ‘ I ‘ - 1 ‘ ‘ I ’ ‘ Tl/Z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #9713: Butane, 1-ethoxy- (CAS) $$ Ethyl butyl ether $$ Eth... 59 TTT • • i ■ • 9.60 9.80 10.00 10.20 5000 m/z 104.00 8.16% 41
-PPPPP-P 73 87 102 niz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #10063: Butanoic acid, 2-hydroxy- $$ Butyric acid, 2-hydro... ■ ■ i • ■ • * i ■ ■ ' ■ i 1 ■ ■ 1 i 1 ■ 31 59 9.60 9.80 10.00 10.20 m/z 73.00 7.91%
5000
45 76
n/z—> ■ i 11 20 -HmH 30 40 50 60I 70 80 104 • ' i ■ ■ ■ ■ i ' * ' ' I 1 ' ' 1 i 1 ■ ■ ■ I ' 1 90 100 110 120 130 ,NA 9.60 9.80 10.00 10.20
>0167.D SCAN508.M Fri Jan 25 10:25:47 2002 Page 11
NYC-WTC_000050495
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NYC-WTC_000050596
Laboratory report listing unknown compounds and surrogate recovery for sample AE00250 analyzed on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050519
Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050539
Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050735
Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050683
Laboratory report listing unknown compounds and surrogate recovery for sample AE00166 analyzed on February 13, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050645
Laboratory report listing unknown compounds and surrogate recovery for sample AE00110 analyzed on February 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051877
GCMS analysis log for sample AE00701 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000050432
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050433
Fragmented page containing a document identifier and instructions regarding liquid-liquid extractor drip rates from January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050435
Gas chromatography-mass spectrometry calibration analysis of sample AE00167 detecting multiple organic compounds including nitrosamines and dichlorobenzenes.
Filed in the same folder
NYC-WTC_000050439
Laboratory report listing concentrations of volatile organic compounds in sample AE00167 analyzed on January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050444
Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.
Filed in the same folder