GCMS report for sample AD28861 showing detection of unknown compounds and surrogate recovery data.
NYC-WTC_000018830–000018848Folder label: “GCMS X 12/17/01 A 12/22 - 12/23/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report • Data File : C:\MSDCHEM\l\5973N\02FEB01\28860.D Vial: 3 Acq On : 1 Feb 2002 12:14 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.17 ug/L 126724 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 59 3 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 53 4 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N60 000945-24-4 53 Abundance Scan 1656 (22.280 min): 28860. D (-) m/z 192.10 100.00% 19/2
5000
— 82 96 146 160 22.00 22.20 22.40 22.60 /z—> 43 70 | 118 128 0 mH —pHHbdtmmmpmmm | I I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 l— m/z 191.10 14.19% Abundance #102588:4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192
108 5000 ' 22.00 22.20 22.40 22.60 146 175 m/z 193.10 14.03% 0- ... 11.,.. | i i i-i p i > 11 (i > i J i rri 11 > 111 > 1111 i'i i । ■1 ■ • । ■1 i1" ■ । ■ • i ■ ■ ■11 • ■' ■ i' 1 ■ i • • “ i n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 1912 I. AAdA 22.00 22.20 22.40 22.60 5000 m/z 146.10 13.94%
96 164
m/z—> 138 0 < i i i j > i i < j i i i i । i i i i । > i i i j i i r i j i j i f p i mTTTTTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 +L TTTTT
Abundance #88409: N-perdeuteriobenzylideneaniline ........... A 1912 22.00 22.20 22.40 22.60 m/z 96.00 13.78% 5000 82
/z—> 0 30 mri... . 54 I 94 110 160 ’ 1—22111T ,. 111.।. 11 rpn 11111 > 111111 n 111 > i ■ > 1111 f j-i 11111111111 i'i1 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 U WU 22.00 22.20 22.40 22.60
28860.D SCAN508.M Mon Feb 04 08:41:05 2002 Page 9
NYC-WTC_000018842
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GCMS laboratory results for sample AE01638 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
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Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared non-person entities · 1 shared topics · similarity 0.996
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Laboratory report showing GCMS analysis results for sample AE00614 conducted on February 1, 2002.
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1 shared non-person entities · 1 shared topics · similarity 0.996
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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
NYC-WTC_000050793
Laboratory report listing unknown compounds and surrogate recovery for sample AE00105 analyzed on February 7, 2002.
Similarity score 0.997 (not a probability)
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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
Similarity score 0.997 (not a probability)
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GCMS laboratory results for sample AE01637 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
Similarity score 0.997 (not a probability)
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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
Similarity score 0.997 (not a probability)
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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
Similarity score 0.997 (not a probability)
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004770
Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.
Similarity score 0.996 (not a probability)
machine-extracted · confidence unavailable · Check page ↗Readers open these alongside this record — through an Ask answer, the same folder, or indexed similarity. Not a claim they are about the same event.
NYC-WTC_000018795
Single-page document containing GCMS data or metadata associated with the WTC site in late December 2001.
Filed in the same folder
NYC-WTC_000018796
Fragmented GCMS data page containing chemical identifiers and numerical values from a December 2001 analysis.
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Calibration report listing response factors and concentrations for multiple organic compounds analyzed on December 22, 2001.
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Reference data report showing measured versus expected values for organic compounds in sample AD29735.
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