Laboratory report listing unknown compounds and surrogate recovery for sample AE00248 analyzed on January 28, 2002.
NYC-WTC_000050558–000050576Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
. Data File : C:\MSDCHEM\1\5973N\02JAN24\00248.D Vial: 4 Acq On : 24 Jan 2002 5:27 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1.. .\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
22.28 0.16 ug/L 121442 Phenanthrene-dl0 22.65
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 52 3 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 49 4 lH-2-Indenone,2,4,5,6,7,7a-hexah... 192 C13H20O 000000-00-0 42 Abundance Scan 1656 (22.280 min): 00248.D (-) m/z 192.10 100.00% 1912
5000i — . k i i i fi r 146 160 82 96
miz—> 42 70 118 1 nmmmmmmmpmmmmpn | 11111111 !■>> 11111111 >> 111111111 ■ 11 > W 11 > i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 l— 22.00 22.20 22.40 22.60 m/Z 96.10 16.39% Abundance #102588:4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192
108 5000 22.00 22.20 22.40 22.60 146 175 m/z 191.10 14.82%
I " ‘' I ‘ “ 1 I' ‘ ‘' I " ‘ I ‘' ‘ ‘ I " '' I ' ' i" " i1 trpu miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192 ............ . 22.00 22.20 22.40 Zi.SD 5000 82 m/z 146.10 14.46%
54 110 30 I 160 94 -HT TTU)mmmpu 11111 m/z—> 20 30 40 50 60 70 80 90 1CX) 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine A mm 1912 22.00 22.20 22.40 22.60 77 151 m/z 193.10 12.63% 130 93 104 5000 119
n-p- 177 'rnTn " ‘ I ■'1 ‘ I' “' I' ‘‘ I' “ ' I • ‘ “ I' ‘ ‘ I ‘ I' ‘'11 “ 118 >’1’>’> J l > I . ( . . . . । . . . ., T T T T m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60
00248.D SCAN508.M Fri Jan 25 10:26:11 2002 Page 13
NYC-WTC_000050574
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NYC-WTC_000050500
Laboratory report for sample AE00168 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052128
Laboratory report showing GCMS analysis of sample AE00843 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052108
Laboratory report showing GCMS analysis of sample AE00840 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052001
GCMS analysis log for sample AE00699 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051984
GCMS analysis log for sample AE00740 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051567
Laboratory report showing GCMS analysis results for sample AE00562 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052069
Laboratory report showing GCMS analysis of sample AE00833 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010027
GCMS laboratory results for sample AE01510 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050432
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050433
Fragmented page containing a document identifier and instructions regarding liquid-liquid extractor drip rates from January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050435
Gas chromatography-mass spectrometry calibration analysis of sample AE00167 detecting multiple organic compounds including nitrosamines and dichlorobenzenes.
Filed in the same folder
NYC-WTC_000050439
Laboratory report listing concentrations of volatile organic compounds in sample AE00167 analyzed on January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050444
Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.
Filed in the same folder