GCMS analysis results for sample AE02713, March 5 2002

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Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02713 including surrogate recovery.

NYC-WTC_000010867–000010886

Folder label: “GCMS X 2/5/02 A 2/28/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\5973N\02FEB28\02713 .D Vial: 3 Acq On : 28 Feb 2002 12:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 3,5-DICHLORO-2-METHOXY-6-ME... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T.

35.38 0.05 ug/L 19382 Perylene-dl2 34.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3,5-DICHLORO-2-METHOXY-6-METHYL-... 207 C7H7C12NO2 000000-00-0 50 2 Phenol, 2,6-dichloro-4-nitro- $$... 207 C6H3C12NO3 000618-80-4 47 3 2-Nitro-4,6-dichlorophenol $$ Ph... 207 C6H3C12NO3 000609-89-2 38 4 2-Chloroaniline-5-sulfonic acid ... 207 C6H6C1NO3S 000098-36-2 9 Abundance Scan 2835 (35.378 min): 02713.D (-) m/z 207.00 100.00% 207 WyW* 5000 133 73 264 281 44 35.00 35.20 35.40 35.60 35.80 oW ' • i 1 ■ ‘ 1 i ■ ■ ■ • i • 1 • ■ I ■ • ■ ■ i ■ ' ■ • i ‘ * i ■ ‘ • i ■ 41484 r। m/z 209.00 59.51% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #125116:3.5-DICHLORO-2-METHOXY-6-METHYL-4-PYRIDINOL 207 177 A 5000 1i 1 1 ■ ■ i ■ ■ ■ ■ i‘ ■ 1 i ■ ‘ ■ i ‘ 35.00 35.20 35.40 35.60 35.80 56 87 142 m/z 132.80 44.94% 73 123 O—TT i ■ ■ ■ ■ i ■ ■ ■ ‘ i ■ ■ ‘ • i ■ ■ • • r■ —+ 164 I I ■ • ■ ■ i ■ ■ ■ । ' i 1 ■ 1 ■ i ■ ■ ' ■ i ' ■ A m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #125086: Phenol, 2,6-dichloro-4-nitro- $$ 2,6-Dichloro-4-n... 267

5000 73 97 125

141 177 pMjvwh ITT 138,8 35.00 35.20 35.40 35.60 35.80

61 161 1 01i■ ■■ ■I ■■■ ■i ■■ 1•i• ■■■i ■■ ■■ I■ ''■ i ■■■ ■i ■ II m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #125091:2-Nitro-4,6-dichlorophenol $$ Phenol, 2,4-dichtor... 207 35.00 35.20 35.40 35.60 35.80 m/z 264.20 35.68% 97 5000 133 62

0■ i■ ■■ •i ■■' 1i 1■ 1■ i■•■■ i ■■ ■ i • ‘ •1 i ■ ' • • i • ‘ ‘ i 1 rnfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 35.00 35.20 35.40 35.60 35.80

02713.D HP022102.M Fri Mar 01 10:06:54 2002 Page 15

NYC-WTC_000010885

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GCMS analysis results, sample AE02719, March 2002 · Box DEP Box 14

NYC-WTC_000010987

Gas chromatography-mass spectrometry analysis of sample AE02719 performed March 5, 2002, reporting other unknown compounds and surrogate 2,4-DDD recovery data.

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