GCMS analysis results for sample AE02713, March 5 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB28\02713 .D Vial: 3 Acq On : 28 Feb 2002 12:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 4-Amino-8-methylimidazo(1,5... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 24.86 0.06 ug/L 33312 Phenanthrene-dl 0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual l 4-Amino-8-methylimidazo(1,5-a)-1... 149 C6H7N5 079681-01-9 4 2 L-Tyrosine, N-acetyl- (CAS) $$ N. . . 223 C11H13NO4 000537-55-3 4 3 5-methyl-7-amino-S-triazolo(1,5-... 149 C6H7N5 033376-96-4 4 4 l-Methyl-5-(trifluoromethyl)pyrrole 149 C6H6F3N 000000-00-0 4 Abundance Scan 1903 (24.857 min): 02713.D (-) m/z 149.00 100.00% 149

5000

41 223 24.60 24.80 25.00 25.20 ob m/z 149.90 5.86% miz-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #44972:4-Amino-8-methylimidazo(1,5-a)-1,3,5-ti1azine $$ 1... 149

5000 ■ ' i ' • ■ ■ i ' • • I ■ ■ • ■ i ' ' 43 24.60 24.80 25.00 25.20 53 122 m/ z 41.10 5.56% 80 96 107 t L ... h.................................. '— ob • ■ । ' । ■ niz-> 20 40 60 80I 100 120 140 160 180 200 220 Abundance #149208: L-Tyrosine, N-acetyl- (CAS) $$ N-Acetyl-L-tyrosin... 149 ‘ * i ■ ■ ■ ■ i ■ ‘ 1 i ■ ■ ■ ■ i ■ 1 24.60 24.80 25.00 25.20 5000 m/z 223.00 4.44%

30

ob 45 7 7 177 t. 223 i miz-> 20 40 60 80 100 120 140 160 180 2(X) 220 Abundance #44982:5-methyl-7-amino-S-triazofo(1,5-A)pyrimidine $$ (1... 149 24.60 24.80 25.00 25.20 m/z 44.05 0.67% 5000

109 , w"*MAWNrnH/n/ 0b • • i • ■ ■ ■ i 1 ' ■ ‘ i ‘ 81 i 95 11134...................... m/z-> 20 40 60 80 100 120 140 160 180 200 220 24.60 24.80 25.00 25.20

02713.D HP022102.M Fri Mar 01 10:06:54 2002 Page 13

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