GCMS analysis results for sample AE02713, March 5 2002

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Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02713 including surrogate recovery.

NYC-WTC_000010867–000010886

Folder label: “GCMS X 2/5/02 A 2/28/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C:\MSDCHEM\1\5973N\02FEB28\02713.D Vial: 3 Acq On : 28 Feb 2002 12:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak. Number 10 N-perdeuteriobenzylideneani... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.10 ug/L 59076 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N-perdeut e ri obenzy1ideneaniline 192 C13D11N 000538-51-2 64 2 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 52 3 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 45 4 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 45 Abundance Scan 1675 (22.283 min): 02713.D (-) 1 m/z 192.00 100.00% 1912

5000

82 96 146 160 _A 22.00 22.20 22.40 22.60

m/z—> 0 »11 * ।।44 I 1 I »i j rp r i 1111 i q : j n j 11 . < । ! I < j i.i i j m । j 11 i q u ri j ul i} i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m Hp m/z 191.00 18.61% Abundance #88409: N-perdeuteriobenzylideneaniline 1912

5000 82 .... 3... 11 22.00 22.20 22.40 22.60 54 110 m/z 146.10 14.81% 30 160 n/z—> 0 111' I'11' 11''111 mHm I 94 mmmmmpmmmp 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine

77 130 151 192 .......As 22.00 22.20 22.40 22.60 93 104 5000 m/z 96.00 14.61% 119

177 A 0- 111115190199311—0010—7——B8T ‘ ‘14 Tp-rr ‘p-TTT Tn-rp- ■ i ■ • “ i ‘ ' • I ■ “11 ■ “ ■ i “ ‘ I ‘ m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102611:2-Propenal, 3-(3,4-dimethoxypheny!)- $$ Cinnamald... ........... I , I i 1912 ‘22.OO 22.20 22.40 22.60 161 m/z 193.00 14.30% 5000 77 149 177 64 89 193 118 138 0- I “ ‘ •I’ * H I . .——.7m—.. TkTumd mmm1__—mg L ICII ....—Il.... ——1—44414 1 ■ i ■1' • i miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

02713.D HP022102.M Fri Mar 01 10:06:54 2002 Page 12

NYC-WTC_000010882

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GCMS analysis results, sample AE02719, March 2002 · Box DEP Box 14

NYC-WTC_000010987

Gas chromatography-mass spectrometry analysis of sample AE02719 performed March 5, 2002, reporting other unknown compounds and surrogate 2,4-DDD recovery data.

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