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GCMS analysis results for sample AE00616, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE00616 conducted on February 1, 2002.

NYC-WTC_000051642–000051659

Folder label: “GCMS X 1/9/02 A 1/29/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN29\00616.D Vial: 5 Acq On : 29 Jan 2002 5:59 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 10 (3s)-3,4-isopropylidendioxy... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T. 26.07 0.07 ug/L 68905 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 (3s)-3,4-isopropylidendioxy-4-me... 174 C9H18O3 067985-68-6 10 2 Heptadecane (CAS) $$ n-Heptadeca... 240 C17H36 000629-78-7 9 3 Nonadecane $$ n-Nonadecane 268 C19H40 000629-92-5 9 4 Hexane, 2,2,3,3-tetramethyl- $$ ... 142 C10H22 013475-81-5 9 Abundance Scan 1988 (26.070 min): 00616. D (-) m/ z 57.10 100.00% 57

5000: 43 AR/Vpww 82 99 141 159 69 119 25.80 26.00 26.20 26.40

n/z-> 40 uf i

60 1 ■ ' ■ 4— i ■

80 100 120 140 160 180 200 220 240 260 m/z 43.10 74.31% Abundance 43 #78522: (3s)-3,4-isopropylidendioxy-4-methylpentan-1-ol Mw/u"WMyok 59 5000 85 ■ ’ i ■ 99 25.80 26.00 26.20 26.40 71 116 159 m/ z 82.10 43.06%

m/z-> Abundance 40

43 60

57 80 100 120 140 160 180 200 220 240 #174554: Heptadecane (CAS) $$ n-Heptadecane $$ Normal-hept... 260 AMAPU/Vna/ 71 25.80 26.00 26.20 26.40 5000 m/z 85.05 41.97% 85

m/z-> Abundance I,, ,il , 40 60 80 ^113 127 100 120 140 160 ......... 180 #211486: Nonadecane $$ n-Nonadecane 200 220 24° 240 260 MMWvNy ' 1 I 1 11 1 I 1 1 1 1 i1 ■ 1 • i 1 ■ 57 25.80 26.00 26.20 26.40 43 71 m/z 79.10 40.30% 85 5000 V

1n 1 113.177 183 197 268 m/z--> 40 100 120 140 160 180 200 220 240 260 25.80 26.00 26.20 26.40

)0616.D SCAN508.M Wed Jan 30 09:02:27 2002 Page 12

NYC-WTC_000051657

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NYC-WTC_000051657Source: NYC Law Department, mirrored locally

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