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GCMS analysis results for sample AE09574, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE09574 conducted on May 14, 2002.

NYC-WTC_000023107–000023121

Folder label: “GCMS X 5/8/02 A 5/9/02

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Scanned page image, NYC-WTC_000023120
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NYC 9/11 Public Portal Document

. Data File C:\MSDCHEM\l\DATA\050902\9574.D Vial: 10 Acq On 9 May 2002 10:37 pm Operator: Mclean Sample 5/8 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 1,4,5,6-Tetrahydro-6-[pheny... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

30.98 0.27 ug/L 337101 Chrysene-dl2 30.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4,5,6-Tetrahydro-6-[phenylmeth... 208 C9H12N4S 1000213-67-4 7 2 Benzene, 1-isocyano-3-methyl- 117 C8H7N 020600-54-8 5. 3 2,4,6-Cycloheptatriene-l-carboni... 117 C8H7N 013612-59-4 4 4 Benzene, l-isocyano-4-methyl- 117 C8H7N . 007175-47-5 5 Abundance Scan 4748 (30.977 min): 9574.D (-4747) (-) m/z 116.00 10 . 00% 1* 6 84 234 103 212 5000 44 ' I ' 1 TI T‘111!‘‘‘I‘I - 30.60 30.80 31.00 31.20 31.40 0 ■ ■ i 1 1 ' ' i m/z 234.10 76.07% /z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #52386:1,4>5,6-Tetrahydro-6-[phenylmethyl]-2H-1,2,4,5-tet... V7

91 5000 "IiT ‘ ‘ I ■ 1 ' 1 I 1 1 30.60 30.80 31.00 31.20 31.40 65 208 m/z 84.00 72.86% 45

m/z-> 0- 1 4 1 ttl1 40 1 155 601 1 80 -+ 100 77 II, , 131I 120 140 103 151 162 177 192 160 TH 180 200 220 240 Abundance #52491: Benzene, 1 -isocyano-3-methyl- 1* 7 nem/MNAturNadr 30.60 30.80 31.00 31.20 31.40 5000 m/z 212.10 68.57% 90

63

0- III I I I II I I" ' 1 ■ i ■ * ................................................................................ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ 1 ■ ■ i ■ 1 ■ ■ i 1 1 1 1 i ■ ■ ■ ■ i 1 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #52120: 2,4,6-Cycloheptatriene-1 -carbonitrile 1' 6 30.60 30.80 31.00 31.20 31.40 90 m/Z 87.90 66.43%

5000

39 51 63 °5 77 0 — ....... 111 .-I 1 1 1 1 ‘ /z-> 40 60 80 100 120 140 160 180 200 220 240 30.60 30.80 31.00 31.20 31.40

9574.D 050102 .M Mon May 13 11:49:49 2002 Page 9

NYC-WTC_000023120

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NYC-WTC_000023120Source: NYC Law Department, mirrored locally

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