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GCMS analysis results for sample AE09575, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE09575 conducted on May 14, 2002.

NYC-WTC_000023130–000023147

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document

- Data File C:\MSDCHEM\l\DATA\050902\9575.D Vial: 11 Acq On 9 May 2002 11:26 pm Operator: Mclean Sample 5/8 kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 8-Azabicyclo[3.2.1]octan-3-... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

29.18 0.27 ug/L 371730 Chrysene-dl2 30.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 8-Azabicyclo[3.2.1]octan-3-ol, 8... 141 C8H15NO 000120-29-6 12 2 Benzocyclodecene, tetradecahydro- 194 C14H26 061142-06-1 12 3 lH-Imidazole, 1-ethyl- 96 C5H8N2 007098-07-9/9 4 2-Cyclopentene-l, 4-dione 96 C5H402 000930-60-9 9 Abundance Scan 4441 (29.173 min): 9575.D (-4438) (-) m/ z 96.10 100< 00% 82 96

au 137 149 42 56 5000 71 207 1 111 28.80 29.00 29.20 29.40 29.60 Omp ‘ ‘I‘ ■ l '' " I PT 1111111'1111"'11" ■11"" I"1 T 1 n [11'11'''11'''' ]''" I''' m/ z 82.10 95.67% iz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #116334:8-Azabicyclo[3.2.1]octan-3-ol, 8-methyl-, endo- 82 96

5000 42 MA, ha, AAAM)A 28.80 29.00 29.20 29.40 29.60 57 67 113124 140 m/z 77.10 74.80% 28 O- '' 'I"" "• 'i" "i ““ i" " i11" i" “ i ' i "■ m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #41792: Benzocyclodecene, tetradecahydro- 916 82 ................. 1 I 1 1 ■ ■ i ■ ■ ‘ I ' ' I ' ' ' ' I ' 55 67 28.80 29.00 29.20 29.40 29.60 41 m/Z 149.00 70.08% 5000

29 109 I 124 138 152 166 180 194

nfe-> 0 ... a.. l...ll,/M 11 " rtlr1111'I" ' ''I " " th > 111 ri 11 > । * ‘ ] 11 > । [ > I > ■ । ।'11 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #41767:1 H-lmidazole, 1-ethyl- 96 28.80 29.00 29.20 29.40 29.60 m/z 137.20 69.69% 81 41 5000 68

54

0 1 - ■m-p- ' i" "i" " i" "I'"' r1" i ■" 'I ' r "' r "' I'" ■ i'" ‘ i1 ‘' ■ i ■ • ■ ■ i TmT Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140150 160 170 180 190 200210 28.80 29.00 29.20 29.40 29.60

9575.D 050102.M Mon May 13 11:51:02 2002 Page 10

NYC-WTC_000023144

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NYC-WTC_000023144Source: NYC Law Department, mirrored locally

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