GCMS analysis results for sample AE09575, May 2002

NYC 9/11 Public Portal Document

• Data File C:\MSDCHEM\l\DATA\050902\9575.D Vial: 11 Acq On 9 May 2002 11:26 pm Operator: Mclean Sample 5/8 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 1-Octadecene Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

29.00 1.46 ug/L 2010140 Chrysene-d12 30.81

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1-Octadecene 252 C18H36 000112-88-9 70 2 1-Nonadecene 266 C19H38 018435-45-5 58 3 1-Heptadecene 238 C17H34 006765-39-5 58 4 11-Tricosene 322 C23H46 052078-56-5/53 Abundance Scan 4412 (29.002 min): 9575. D (-4397) (-) m/z 55.10 100/00%! 55

43 — 83 97 5000 69 111 127 28.60 28.80 29.00 29.20 29.40

/z-> O—TTTT 20 40 T[3 60 .4.1,4141.+167179193207 80 100 120 140 160 180 200 220 240 260 m/z 43.15 59.74% Abundance #112298:1 -Octadecene 43 57 83 69 97

5000 29 111 28.60 28.80 29.00 29.20 29.40 125 m/z 57.10 57.05%|

niz-> 0- 1' i 1,11111 20 40 UM X 11113.182.154/168 182,196210,224. 60 80 252 ' I' ' i " 100 120 140 160 180 200 220 240 260 Abundance #42210:1-Nonadecene 43 55 83 9|7 WWAwAA) 69 111 28.60 28.80 29.00 29.20 29.40 5000 m/ z 83.10 52.11% 125 29 1 139 154 168 182 196 210 224 238 266 0- 15 , ,,[! ' ' I ' 1 ' ‘T1 + T-p J r , 4 , , ft | p , , r, । ri । । ri । । ■ । । I1, । । i i । , n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #118308:1 -Heptadecene I ‘ • i • ■ .........................

□ 43 55 69 83 97 28.60 28.80 29.00 29.20 29.40 50.27%| 111 5000

29 125 J5 1 , Il+— 0 1 1 1 f ' 1 * 'T1 । 139 154 168 182 196 210 111 i "rfmiI P . ........... . 238 1 ■ i ' ■ ■ 1 i ' ■ -nfz.-> 20 40 60 80 100 120 140 160 180 200 220 240 260 28.60 28.80 29.00 29.20 29.40

9575.D 050102.M Mon May 13 11:51:01 2002 Page 9

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