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GCMS analysis results for sample AE09575, May 2002

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Laboratory report showing GCMS analysis of sample AE09575 conducted on May 14, 2002.

NYC-WTC_000023130–000023147

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document

- Data File C:\MSDCHEM\l\DATA\050902\9575 .D Vial: 11 Acq On 9 May 2002 11:26 pm Operator: Mclean Sample 5/8 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 8 Benzoic acid, p-anilino-, m.. Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 31.38 0.37 ug/L 503791 Chrys ene-d12 30.81 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, p-anilino-, methyl... 227 C14H13NO2 004058-18-8 14 2 1,2-Benzenedicarboxylic acid, mo... 278 C16H2204 004376-20-9 14 3 1,2-Benzenedicarboxylic acid, mo... 278 C16H2204 004376-20-9 14

A 4 Oxazolidine, 3-phenyl- 149 C9H11NO 020503-92-8/10 Abundance Scan 4817 (31.382 min): 9575.D (-4810) (-) m/z 227.20 100/00% 149 227

57 5000 113 41 70 167 197 ' i ' ■ 1 ’ i ' ■ 31.00 31.20 31.40 31.60 31.80 LMlua,— 0 il m/z 149.00 96.32% ] ■ ' 1 ■ I'1 1 1 ’ 11 ' n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #89099: Benzoic acid, p-anilino-, methyl ester 227 196

5000 ... A ■ i ■ ■ 1 ■ i■

31.00 31.20 31.40 31.60 31.80 ■ LMnpul 167 m/z 57.10 50.13%| 51 65 77 98 115 139 ,. 180 O+ I 1 ' ' ' M " no 'I . ... r— Hr । । rn ।। । । । । i /’’’’I’ ■ ’ill . 1 1 .1 . » I > I m/z-> :20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #67064:1,2-Benzenedicarboxylic acid, mono(2-ethylhexyl) este 149

31.00 31.20 31.40 31.60 31.80 5000 m/z 113.50 41.44%| 70 167 29 41 55 83 112 132 | 199 213 228 242 256 278 01rTr। 'li i II, phall. llmlya , %7 [1.,. ,|., 1, —TI 1 ■ ' 185 i ■ ' ■ 1 i ■ 1 ' ' i ' ■ ‘ ' i • ■ ■ ■ i • 1 ■ ‘'i ■ ' m/z-> :20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #123456:1,2-Benzenedicarboxylic acid, mono(2-ethylhexyl)... 1 1 ' 1 1 1 i ‘ 1 ■ ■ i ■ ■ 149 31.00 31.20 31.40 31.60 31.80 m/z 226.00 31.91%| 5000 70 57 167 41 83 112 ........ ).. 0 rp . । i । । । i t । । । "j । । "i । i*— 1l ........ l. 140 ‘120 ...................... 279 ' i 1 1 ■ ' i 1 ■ 1 ' i 1 1 I ' 1 1 1 1 ' 1 m/z-> 20 40 60 80 100 160 180 200 220 240 260 280 31.00 31.20 31.40 31.60 31.80

9575.D 050102.M Mon May 13 11:51:02 2002 Page 11

NYC-WTC_000023145

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NYC-WTC_000023145Source: NYC Law Department, mirrored locally

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