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GCMS analysis results for sample AE09575, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE09575 conducted on May 14, 2002.

NYC-WTC_000023130–000023147

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document

.Data File : C:\MSDCHEM\l\DATA\050902\9575.D Vial: 11 Acq On : 9 May 2002 11:26 pm Operator: Mclean Sample : 5/8 kb Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 5-Thiazolecarboxylic acid, . Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

33.84 0.57 ug/L 572763 Perylene-dl2 34.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 5-Thiazolecarboxylic acid, 2,4-d... 185 C8H11N02S 007210-77-7 50 2 dl-2-Ethylhexyl chloroformate 192 C9H17C102 024468-13-1 27 3 Benzene, l-nitro-2-(octyloxy) - 251 C14H21NO3 037682-29-4 17 4 Benzene, l-nitro-2-(octyloxy) - 251 C14H21NO3 037682-29-4 17 Abundance Scan 5235 (33.838 min): 9575.D (-5227) (-) m/z 185.10 100.00% 185

57 5000 71 43 84 98 112 125139 , . th . 33.60 33.80 34.00 34.20 — 281 203 O-m —l— JJIiL i ■ ■ ■ ■ i 1 IIi............... -- I m/z 57.10 57.14% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #79017:5-Thiazolecarboxylic acid, 2,4-dimethyl-, ethyl ester ___ 140 185

71 A-NWWwwj 5000 116 157 45 33.60 33.80 34.00 34.20 98 m/z 71.10 44.73%

m/z-> O- 20 40 60 80 L.178.1., h III I 1 1 1 1 1 11>'I ■ ' ■ ' I ' ' ' ' I ’'1'I'' ' ' I ' ' 100 120 140 160 180 200 220 240 260 280 Abundance 57 70 #17577: dl-2-Ethylhexyl chloroformate 112 mosoutootsa 33.60 33.80 34.00 34.20 5000 m/z 70.10 40.83% 43 83

01........ " panll—44 97 । li"il"| । (al 129 149... 192................. m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #16294: Benzene, 1 -nitro-2-(octyloxy)- 43 57 33.60 33.80 34.00 34.20 m/z 43.15 33.81% 71 5000 29 83 112 139 MpMWlhwr — 221 251 m/z-> 0 : 20 40 1444 +41 60 80 .27,1,174.,.., ■ । > > 1 ■ । 100 120 140 160 180 200 220 240 260 280 ■ 1 1 । > 1 1 । l' 1 1 1 > । । - 33.60 33.80 34.00 34.20

9575.D 050102.M Mon May 13 11:51:02 2002 Page 12

NYC-WTC_000023146

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NYC-WTC_000023146Source: NYC Law Department, mirrored locally

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