NYC 9/11 Public Portal Document
.Data File : C:\MSDCHEM\l\DATA\050902\9575.D Vial: 11
Acq On : 9 May 2002 11:26 pm Operator: Mclean
Sample : 5/8 kb Inst Instrumen
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
*********************************************************************
Peak Number 9 5-Thiazolecarboxylic acid, . Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
33.84 0.57 ug/L 572763 Perylene-dl2 34.71
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 5-Thiazolecarboxylic acid, 2,4-d... 185 C8H11N02S 007210-77-7 50
2 dl-2-Ethylhexyl chloroformate 192 C9H17C102 024468-13-1 27
3 Benzene, l-nitro-2-(octyloxy) - 251 C14H21NO3 037682-29-4 17
4 Benzene, l-nitro-2-(octyloxy) - 251 C14H21NO3 037682-29-4 17
Abundance Scan 5235 (33.838 min): 9575.D (-5227) (-) m/z 185.10 100.00%
185
57
5000 71
43
84 98
112
125139 ,
. th .
33.60 33.80 34.00 34.20
— 281 203
O-m —l— JJIiL
i ■ ■ ■ ■ i 1
IIi............... --
I m/z 57.10 57.14%
m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280
Abundance #79017:5-Thiazolecarboxylic acid, 2,4-dimethyl-, ethyl ester ___
140 185
71 A-NWWwwj
5000 116 157
45 33.60 33.80 34.00 34.20
98 m/z 71.10 44.73%
m/z->
O-
20 40 60 80
L.178.1., h III
I 1 1 1 1 1 11>'I ■ ' ■ ' I ' ' ' ' I ’'1'I'' ' ' I ' '
100 120 140 160 180 200 220 240 260 280
Abundance
57 70
#17577: dl-2-Ethylhexyl chloroformate
112 mosoutootsa
33.60 33.80 34.00 34.20
5000 m/z 70.10 40.83%
43 83
01........ " panll—44 97 । li"il"| । (al
129 149... 192.................
m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280
Abundance #16294: Benzene, 1 -nitro-2-(octyloxy)-
43 57 33.60 33.80 34.00 34.20
m/z 43.15 33.81%
71
5000
29 83 112
139
MpMWlhwr
— 221 251
m/z->
0
:
20 40
1444 +41
60 80
.27,1,174.,.., ■ । > > 1 ■ ।
100 120 140 160 180 200 220 240 260 280
■ 1 1 । > 1 1 । l' 1 1 1 > । । -
33.60 33.80 34.00 34.20
9575.D 050102.M Mon May 13 11:51:02 2002 Page 12
NYC-WTC_000023146
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