GCMS analysis results for sample AE08756, May 2002

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Laboratory report documenting GCMS analysis of sample AE08756 conducted on May 8, 2002.

NYC-WTC_000044731–000044747

Folder label: “GCMS X 4/29/02 A 5/3/02”

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NYC 9/11 Public Portal Document

- Data File C:\MSDCHEM\l\DATA\050202\8756.D Vial: 15 Acq On 2 May 2002 11:05 pm Operator: Mclean Sample 4/29 re-ext Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.49 ug/L 499240 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Anthracene-diO- 188 C14D10 001719-06-8 94 2 Phenanthrene-diO 188 C14D10 001517-22-2 94 3 Pentacyclo[7.3.1.1. (4,12) .0(2,7) .. . 188 C14H20 1000215-61-8 45 4 1,3,5-Triazin-2-amine, 4,6-bis(m... 188 C5H8N4S2 030358-19-1 38 Abundance Scan 3409 (23.109 min): 8756.D (-3402) (-) m/z 188.15 100.00% 188

5000 ....................... .............................. 80 94 160 22.80 23.00 23.20 23.40 43 52 66 , m/z-> mummP—Th al......... 132,146 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 p Tun m/ z 80.10 15.70% Abundance #79826: Anthracene-d10- 188

5000 1 ' i ' । । । । i-1 । [ i r 22.80 23.00 23.20 23.40 m/Z 189.10 14.87% — 80 94 160 , 11 17 30 42 52 66 J J 108 118 132 i । । ri-rp । । । । । । rfoogtk । । p I I । p ■ I I । I । i I | I I । । | t ri FTI rr i TITTTJ 11 r 146—170179 —— TI n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/z 94.15 13.68%

80 94 160 30 42 52 66 i । । I J 111I rr p r108 । p ■ > i p < । i p i । i p i । i । I I । । p I I । p i rl i i [ i i i i p i i i | I I i +146—4179179—— 118 132 17 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3.1.1.(4,12).0(2,7).0(6,11)]tetradeca... 1 r i 1 ' ■ ' 1 ‘ 1 । 1 1 1 ' i 1 ' 1 1 i 188 22.80 23.00 23.20 23.40 m/z 184.10 13.09%

5000 79 91 55 67 131 105 117 — Hl.+ ji 1 — 145 ’T’TII’’ > rp । . । । . - 159.173 . ...... 1 | 1 1 1 ' rq ■ r. । p । > > । ’ ’ ’I’UU 110111 i_ ।' ।' iii i j । । ~I । ] i । । । । । । /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180190 22.80 23.00 23.20 23.40

8756.D 050102.M Mon May 06 14:03:06 2002 Page 12

NYC-WTC_000044746

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NYC-WTC_000044746Source: NYC Law Department, mirrored locally

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