GCMS blank analysis results, sample AE10809, May 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\051402\0507LB.D Vial: 16 Acq On : 15 May 2002 2:34 am Operator: Mclean Sample : 5/7 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHGDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Cyclohexasiloxane, dodecame... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

15.48 2.92 ug/L 2640020 Napthalene-d8 13.43

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexasiloxane, dodecamethyl- 444 C12H36O6S16 000540-97-6 87 2 Cyclohexasiloxane, dodecamethyl- 444 C12H36O6Si6 000540-97-6 80 3 1,1,1,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 32 4 Guaifenesin di-tms derivative 342 C16H30O4Si2 1000137-06-7 17 Abundance Scan 2111 (15.483 min): 0507LB.D (-2101) (-) m/ z 73.10 100.00% 73

5000 341 147 > । । — । । i> i । । । । । । । । । 429 15.20 15.40 15.60 15.80 45 179 207 251 281 311 [ 0- ।__ L 1 । 1 117 TIl r ' ।' ~ I j । i । i । । । । i । > । 1 i 1 397,— m/z 341.00 36.17% /z-> 50 100 150 200 250 300 350 400 Abundance #27931: Cyclohexasiloxane, dodecamethyl- 73 341

429 5000 *111111 1"’*’ 11 1 1 " 11 1 15.20 15.40 15.60 15.80 147 m/z 147.10 19.71% 45 117 [ 207 267 311 [ 397 01 I —I— !' । | ■ 1 — 1dl 1 1 ' m/z-> 50 100 150 200 250 300 350 400 Abundance #115309: Cyclohexasiloxane, dodecamethyl- 73 ...... n....... ■ ■ ।11 ■' । ■ ■' ■ । ■1'' ।11 15.20 15.40 15.60 15.80 5000 m/z 429.10 12.17% 341 429 147 26 45 98 117 | 177 207 251 271 292311 L i 367 397 0 T—' 11 1 | I I I | ! ! I ' ll ' I 1 Tid Tl m/z-> 50 100 150 200 250 300 350 400 Abundance #26950: 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)... 73 15.20 15.40 15.60 15.80 m/z 342.00 11.25% 147 5000 267 355 429 45 207

/z-> 0 50 1 100 l Tl 150 1 ' 200 i 1 L ' ‘ 'I 250 ' 300 'i' 350 — 400 15.20 15.40 15.60 15.80

0507LB.D 050102.M Thu May 16 12:35:54 2002 Page 9

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