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GCMS analysis results for sample AE00556, Feb 2002

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Laboratory report showing GCMS analysis results for sample AE00556 conducted on February 1, 2002.

NYC-WTC_000051549–000051566

Folder label: “GCMS X 1/9/02 A 1/29/02

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NYC 9/11 Public Portal Document

Data File: C:\MSDCHEM\1\5973N\02JAN29\00556.D Vial: 3 . Acq On : 29 Jan 2002 12:12 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 8 Nonanal (CAS) $$ n-Nonanal ... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

11.65 0.14 ug/L 84542 Naphthalene-d8 13.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Nonanal (CAS) $$ n-Nonanal $$ n-... 142 C9H180 000124-19-6 78 2 Nonanal (CAS) $$ n-Nonanal $$ n-... 142 C9H180 000124-19-6 53 3 l-Heptene (CAS) $$ 1-n-Heptene $... 98 C7H14 000592-76-7 49 4 l-Heptene $$ n-Hept-l-ene $$ 1-n... 98 C7H14 000592-76-7 49 Abundance Scan 725 (11.651 min): 00556. D (-) m/z 57.10 100.00% 57 41

5000 70 82 98 —A— 11.40 11.60 11.80 12.00

m/z--> • l ■ . ■ ' I ■ 20 30 40 .1,11,4944 50 60 70 80 90 100 -P 110 T-J—r-t-r-r-j-f—r-r-f—p-r 120 m/z56.10 74.74% Abundance #38509: Nonanal (CAS) $$ n-Nonanal $$ n-Nonylaldehyde $$ N... 41 57

5000 27 70 11.40 11.60 11.80 12.00 82 m/z 41.10 69.56% 98 34 • i ■ • ■ ■ i • > • • । l ■ • i ■ • ■ i • • ... 'll... . miz-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #38524: Nonanal (CAS) $$ n-Nonanal $$ n-Nonylaldehyde $$ N... 57 8000 41 ...A. AAA,,.., 11.40 11.60 11.80 12.00 6000 m/z 43.10 63.54%

4000 70 98........... ' I ' ' ' ' I ’ ' ' ' 1 1 nil /z-> 20 30 40 60 70 80 90 100 110 120 Abundance 50 #7327:1-Heptene (CAS) $$ 1-n-Heptene $$ n-Hept-1-ene $$ h... A A A/ AMY 41 56 11.40 11.60 11.80 12.00 m/z44.10 57.12%

5000 70 98

■ i ■ ■ 1 ■ i ' 1 ' ’ । P4 ' i . ' 1 83 I..... AA.N,A..A.AA....0 m/z—> 20 30 40 50 60 70 80 90 100 110 120 11.40 11.60 11.80 12.00

)0556.D SCAN508.M Wed Jan 30 09:01:58 2002 Page 10

NYC-WTC_000051562

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NYC-WTC_000051562Source: NYC Law Department, mirrored locally

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