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GCMS surrogate recovery results for sample AE00278, Jan 2002

Machine-extracted title · confidence 90%

Laboratory record documenting GCMS surrogate recovery data for sample AE00278 analyzed on January 10, 2002.

NYC-WTC_000050856–000050874

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050872
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02JAN09\278.D Vial: 3 Acq On 9 Jan 2002 7:50 pm Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Nonadecane (CAS) $$ n-Nonad... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

35.74 0.11 ug/L 88498 Perylene-dl2 34.42

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 72 2 Tetratriacontane $$ n-Tetratriac... 479 C34H70 014167-59-0 72 3 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 64 4 Docosane $$ n-Docosane $$ Normal... 310 C22H46 000629-97-0 64 Abundance Scan 2835 (35.741 min): 278.D (-) m/ z 57.05 100.00% 57 85 5000

Aw, w h, N

_u 113133 35.40 35.60 35.80 36.00 207 281 m/ Z 43.10 66.10% 0 ■ ■ । ■" ”i1 >t" • 11*'■ ■ i'"■ i•" • i"■ ■ i"i• • > ■ ■ ■ • i■ " ■ i" "i • * • ’ i1"• i" ’' i "'' i m/z-> 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #211484: Nonadecane (CAS) $$ n-Nonadecane 57

5000 85 35 40 35.60 35.80 36.00 m/ z 71.10 61.86% A m/z-> Hli1!1 141 0 ■ ‘ i1" j " " ir 241 298 rn'I■"•I 1' I' " • I •'" I" u l 40 60 80 100120140160180200 220 240 260 280 300 320 340 360 380 400 r ” ■i i" ' ‘ I

Abundance #363627: Tetratriacontane $$ n-Tetratriacontane F7

AMA.. AA 35.40 35.60 35.80 36.00 5000 85 m/z 85.10 59.71%

mlz-> 1 1313.141,169/ O-m 1’11’1’EE03rT0—B1—E"TT"TTTT 367 i" " i 410 11) i" " i" ■' i'k" i" " i 40 60 80 100 120140 160 180 200 220 240260 280 300 320 340 360 380 400 I 311 I

Abundance #245745: Heneicosane $$ n-Heneicosane A' 1, I’M’ 'A , ' I' ' ' ' ' I ' ' ' 57 35.40 35.60 35.80 36.00

Man m/ Z 55.10 25.73% 85 5000

113 .. J । 141 , 268 296 0 " i" '11' r "d i" " r " ■ r " ■ r " ' r " ■ r "' r "' r " 1 r " • i" " i'1" i"'11H 111" " I m/z-> 40 60 80 100 120140 160 180 200 220 240260 280 300 320 340 360 380 400 35.40 35.60 35.80 36.00

278.D SCAN508.M Thu Jan 10 11:51:45 2002 Page 12

NYC-WTC_000050872

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NYC-WTC_000050872Source: NYC Law Department, mirrored locally

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