GCMS analysis results, sample AE00738, January 2002

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Llprary search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN16\00738.D Vial: 6 Acq On : 16 Jan 2002 7:17 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Nonadecane (CAS) $$ n-Nonad... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 34.12 0.24 ug/L 115310 Perylene-dl2 34.42 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 72 2 Octacosane $$ n-Octacosane 394 C28H58 000630-02-4 72 3 Nonadecane 268 C19H40 000629-92-5 64 4 Hexatriacontane 507 C36H74 000630-06-8 64 Abundance Scan 2693 (34.119 min): 00738. D (-) m/z 57.10 100.00%

_N 57

85 5000

AAAAMMAAMY 207 33.80 34.00 34.20 34.40 0 Tn TTT m/ Z 71.10 74.39% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #211483: Nonadecane (CAS) $$ n-Nonadecane 57

5000 85 ... hw . w 33.80 34.00 34.20 34.40 m/ z 43.10 66.21% , J 113 | 141 183 211 240 268 0 "I "I TT 0u——uun‘‘00‘mna‘—*0——u—mnuuf"—ITuu‘ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #329266: Octacosane $$ n-Octacosane 57 MWAA, A 33.80 34.00 34.20 34.40 5000 85 m/z 85.10 53.90%

/z-> 0 T ■ i " " I' .l 169 196 224 281 350 394 ■ i "" i'‘" 11"" i1' " i" " i " " f1" 11" " I " ITT’ '111" " i " " i ■ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance 57 #211481: Nonadecane ' 1 I ' 1 33.80 34.00 34.20 34.40 4 m/z 55.10 26.41%

5000 85

m/z-> 0 111111 T’’ 18.1(1,169, 224 'I1'"! 268 TTT 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 r •" i ■ " 11" " r " ' i " " r IN 33.80 34.00 34.20 34.40

10738.D SCAN508.M Thu Jan 17 08:17:48 2002 Page 13

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