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GCMS analysis results, sample AE00738, January 2002

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Gas chromatography-mass spectrometry analysis of sample AE00738 conducted on 1/29/02, detecting unknown compounds and 2,4-DDD surrogate at 99 ug with 5.0 MDL.

NYC-WTC_000051948–000051966

Folder label: “GCMS X 1/10/02 A 1/16/02

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NYC 9/11 Public Portal Document

LLDrary bedrcn compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN16\00738.D Vial: 6 • Acq On : 16 Jan 2002 7:17 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 12 Dotriacontane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 34.93 0.20 ug/L 96347 Perylene-dl2 34.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dotriacontane 451 C32H66 000544-85-4 72 2 Octadecane 254 C18H38 000593-45-3 53 3 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 50 4 Decane, 2,9-dimethyl- $$ 2,9-Dim... 170 C12H26 001002-17-1 50 Abundance Scan 2764 (34.930 min): 00738.D (-) m/z 57.10 100.00% F7

5000 85

m/z-> o1 LL 50 100 150 200 250 300 350 400 450 34.60 34.80 35.00 35.20 m/z71.10 77.10% Abundance #355041: Dotriacontane 43

5000 71 —M 14— 34.60 34.80 35.00 35.20 m/z 43.10 54.79%

O-T J 1,7127,1554183 —

L 379 407 450 /z-> 50 100 150 200 250 300 350 400 450 Abundance #193179: Octadecane 57 C4 I W ' 1 1 1 1 1 1 1 1 ' ' ' I 34.60 34.80 35.00 35.20 5000 m/ z 85.10 45.62% 85

113,141 169 226 254 O-T ——————— m/z-> 50 100 150 200 250 300 350 400 450 .. Abundance #113303: Tetradecane (CAS) $$ n-Tetradecane $$ Isotetradecane 1 1 11171 I 1 1 1 1 1 57 34.60 34.80 35.00 35.20 m/z 55.10 31.09%

m/z-> 5000

0 T 50 85

1113.141 100 150 198 200 250 300 350 400 450 Yi 34.60 34.80 35.00 35.20

)C738.D SCAN508.M Thu Jan 17 08:17:48 2002 Page 14

NYC-WTC_000051965

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NYC-WTC_000051965Source: NYC Law Department, mirrored locally

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