GCMS surrogate recovery results for sample AE00278, Jan 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN09\278.D Vial: 3 Acq On 9 Jan 2002 7:50 pm Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 9 Hexatriacontane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 34.94 0.14 ug/L 110239 Perylene-dl2 34.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 72 2 10-Methylnonadecane 282 C20H42 056862-62-5 72 3 Pentatriacontane 493 C35H72 000630-07-9 72 4 Triacontane 422 C30H62 000638-68-6 72 Abundance Scan 2765 (34.941 min): 278.D (-) m/z 57.10 100.00%

C 43 57 71 85

5000

— 113 193 34.60 34.80 35.00 35.20 0 । ■ ■ ■ ■ । I.. /208... m/ z 43.10 78.71% /z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #369896: Hexatriacontane 43 57

71 5000 85 MWWVAAA TT1 34.60 34.80 35.00 35.20 07 m/ z 71.10 69.67%

/z-> 01TTTrT 40 Trrr IT 60 80 1411 127141155 196 210 225 239 253260267 280 100 281 T+0UTOTTTTT 120 140 160 180 200 220 240 Abundance #229010:10-Methylnonadecane 57

71 (. rJ...... A..) 85 34 60 34.80 35.00 35.20 5000 m/z 85.10 66.15%

99 154 42 .1 113126 0 I ' ''"I ' i “ LI ii ii. m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 43 57 #367079: Pentatriacontane AAA —AMIAAN 34.60 34.80 35.00 35.20 m/z 55.00 24.63% 71 5000 85

97 0 Tvn—rf । , I , 11 .1'1, 113.127 141 155 169 183 197 211 225 239 /z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 34.60 34.80 35.00 35.20

278.D SCAN508.M Thu Jan 10 11:51:45 2002 Page 11

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