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GCMS analysis results for sample AE01141, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01141 conducted on February 27, 2002.

NYC-WTC_000003543–000003562

Folder label: “GCMS X 1/20/02 A 2/25/02

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NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02FEB25\01141.D Vial: 7 Acq On : 25 Feb 2002 4 :11 pm Operator: , ’ Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Tetracosane Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

19.92 0.07 ug/L 46412 Acenaphthene-dl0 18.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1 64 2 Octacosane 394 C28H58 000630-02-4 64 3 Dotriacontane 451 C32H66 000544-85-4 64 4 Pentatriacontane 493 C35H72 000630-07-9 64 Abundance Scan 1466(19.923min): 01141.D(-) m/ z 57.10 100.00% 57

5000 85 A TUI 1 ' I 1 1 1 ' [ ■ 1 i 164 19.60 19.80 20.00 20.20

■n/z-> 0! — 50 1 100 I............ *1*‘I 150 200 250 300 350 400 450 m/z 43.10 71.01% Abundance #288784: Tetracosane 57

5000 85 171’’‘ W 19.60 19.80 20.00 20.20 m/z 71.10 58.71%

0l33 1 , J, 1113.141 . , , 197 225 294 . ....... m/z-> 50 100 150 200 250 300 350 400 450 Abundance #329267: Octacosane 7

19.60 19.80 20.00 20.20 5000 m/z 85.10 46.71% 85

y 113,141 169 197 225 394 O—r ■ i ‘ ' i'' ' ■ 'i 1 ''' ' i ' ' ' ' i ' ' ' ' i ' 1 ' ' i ' ' ' ' i ' m/z-> 50 100 150 200 250 300 350 400 450 Abundance #355040: Dotriacontane - 57 19.60 19.80 20.00 20.20 m/z 41.10 26.33%

5000 85

O—r I 1113,141 196 281 422 450 1 ' i * 1 1 1 i ' ■ ■ ■ i ■ ■ ■ 1 I mfe-> 50 100 150 200 250 300 350 400 450 19,60 19.80 20.00 20.20

01141.D HP022102.M Tue Feb 26 08:30:26 2002 Page 9

NYC-WTC_000003555

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NYC-WTC_000003555Source: NYC Law Department, mirrored locally

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