GCMS analysis results for sample AE00555, Feb 2002

NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02JAN29\00555.D Vial: 1 . Acq On : 29 Jan 2002 2:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Cyclopentasiloxane, decamet... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

12.54 0.10 ug/L 73429 Naphthalene-d8 13.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 78 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 42 3 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 36 4 N-(Trifluoroacetyl)-N,O,O',O''-t... 553 C22H42F3NO4Si4 000000-00-0 28 Abundance Scan 803 (12.542 min): 00555.D (-) "2 73.10 100.00% 73

5000 267 355 ----------------- 45 193 | 12.20 12.40 12.60 12.80 ,i. ' i --------- 1 i 1 1 1 1 । 1 m/z 267.00 36.22% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 ' I 1 ' ' 1 T ' 1 11 1 1 12.20 12.40 12.60 12.80 m/z 355.10 31.63%

■ । ....... 207 323 | /z-> 50 100 150 200 250 300 350 400 450 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

12.20 12.40 12.60 12.80 5000 267 m/z 356.10 13.92% 355 45 j~ i , 193 223 . m/z—> 50 — ————————— 100 150 200 250 ■ 300 323 1350/ 400 450 Abundance #361626: Benzeneacetic acid, .alpha.,3,4-tris[(trimethylsi... 1 ■ i ■ ■ ■ 1 I ■ ■ ■ i ■ » ■ ■ । ‘ 1 73 12.20 12.40 12.60 12.80 m/z 74.00 10.25%

5000 355 45 147 [ 193 267 295 1 429 457 i ■ ' I 1 ■ । TTT I । ' 1 1 1 I rl — m/z—> 50 100 150 200 250 300 350 400 450 12.20 12.40 12.60 12.80

)0555.D SCAN508.M Wed Jan 30 09:01:52 2002 Page 9

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