GCMS analysis results for sample AE00555, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN29\00555.D Vial: 1 . Acq On : 29 Jan 2002 2:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************* * * * * ******************** Peak Number 8 Imidazole-2,4,5-d3 $$ lH-Im... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 19.99 0.04 ug/L 30382 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Imidazole-2,4,5-d3 $$ lH-Imidazo... 71 C3HD3N2 006745-43-3 9 2 3-PENTEN-2-OL, (Z)- 86 C5H10O 024652-50-4 7 3 3-Penten-2-ol (CAS) $$ 2-PENTEN-... 86 C5H10O 001569-50-2 7 4 3-Penten-2-ol $$ .alpha.,.gamma.... 86 C5H10O 001569-50-2 7 Abundance Scan 1455 (19.985 min): 00555.D (-) m/z 71.00 100.00% 7h

43 149 5000

111 ................. I 86 | 19.60 19.80 20.00 20.20 20.40 - m/z 43.10 51.39% ‘it 1 1 1 ' 1 1 I ■ ■ ■ 1 i ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #1086: lmidazole-2,4,5-d3 $$ 1 H-Imidazole-2,4,5-d3 (CAS) $... 7h

43

5000 19.60 19.80 20.00 20.20 20.40 m/z 149.10 47.19% I n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #4208: 3-PENTEN-2-OL, (Z)- 7h 43 11 i ' 1 I ’ ’ ' ' I ’ ' 1 1 I ' ' 19.60 19.80 20.00 20.20 20.40 5000 m/z 44.00 21.14% 53 27 M )

m/z-> 20 ■ i ' ■' ' i ■ ' 30 40 ll 11 " 1 I 1 1 । 1 I 1 1 50 60 70 80 86 90 100 110 120 130 140 150 Abundance #4045: 3-Penten-2-ol (CAS) $$ 2-PENTEN-4-OL $$ Methyl prop... TI -r-r-j-r-r | • ■ • " | • • ■ • | • 71 19.60 19.80 20.00 20.20 20.40 m/ z 41.10 19.90% 43 5000

53 86 ■ i1 1' 11 ' ' ' ' I I 1 i . I) — PTTpr ' i 1 ' 1 ' i ' ' 1' I’1 r 11′1 /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 19.60 19.80 20.00 20.20 20.40

)0555.D SCAN508.M Wed Jan 30 09:01:52 2002 Page 10

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