GCMS analysis results for sample AE03185, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03185 conducted on March 15, 2002.

NYC-WTC_000006065–000006084

Folder label: “GCMS X 2/12/02 A 3/01/02”

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Data File : C:\MSDCHEM\1\5973N\02MAR01\03185.D Vial: 5 ’ Acq On 1 Mar 2002 1:38 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Imidazole-2,4,5-d3 $$ lH-Im... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 5.02 0.07 ug/L 25289 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Imidazole-2,4,5-d3 $$ IH-Imidazo... 71 C3HD3N2 006745-43-3 7 2 Acetaldoxime $$ (E) -CH3CH=NOH $$... 59 C2H5NO 000107-29-9 7 3 (Aminomethyl )cyclopropane 71 C4H9N 002516-47-4 4 4 1-Propanamine (CAS) $$ n-Propyla... 59 C3H9N 000107-10-8 4 Abundance Scan 146 (5.022 min): 03185.D (-) m/ z 71.00 100.00% 71 43

5000 59 55 51 4.60 4.80 5.00 5.20 5.40 0 1 11 I l ■ ■ ■ - i ■ 1 ■ ■ 11 ■ ■ • i ■ m/ z 43.10 82.19% m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #1085: lmidazole-2,4,5-d3 $$ 1 H-lmidazole-2,4,5-d3 (CAS) $... 71

5000 43 MAAMA 4.60 4.80 5.00 m/z 41.10 5.20 5.40 54.32% 16 27 30 40 | | ol i 1 1 ' ' i '' ' 11 1 ' ' 1 i ' i r I | I I i I | I I I T j i i H | I I I I | | | | ■ । ■ ■ ■ ■ । ' i 1 I । i । । 11 i68i 11 11111TIT1 A n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #644: Acetaldoxime $$ (E)-CH3CH=NOH $$ Acetaldehyde oxime ... 15 59 41 44 4.60 4.80 5.00 5.20 5.40 5000 rn/z 59.10 38.37% 27 30 Of13 — Lh3?.... i ■''' i''1' i " I ■ ■ ■ ■ ।'11 ‘ i ■ ■ ■ ■ ।' ■' ■ । ■ miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #1489: (Aminomethyl)cyclopropane N r1^ MAA 43 4.60 4.80 5.00 5.20 5.40 30 m/ z 69.10 38.13%

5000

71 27 ■ 111 ■ ■ ■ । ■ ■ ■ • । 68 ■ 54 । 1 1 11 34 38 ] 111 11 > > । 11 1 0 ' ■ ''I ■11' l ■ । Pri i m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 4.60 4.80 5.00 5.20 5.40

'3185.D HP022102.M Mon Mar 04 12:33:00 2002 Page 9

NYC-WTC_000006077

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