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GCMS analysis results for sample AE00555, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE00555 conducted on February 1, 2002.

NYC-WTC_000051531–000051548

Folder label: “GCMS X 1/9/02 A 1/29/02

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Scanned page image, NYC-WTC_000051545
OCR text

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NYC 9/11 Public Portal Document

2 DcaLtis toupoulU RCPOL L

Data File : C:\MSDCHEM\1\5973N\02JAN29\00555.D Vial: 1 Acq On : 29 Jan 2002 2:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************** ** **** * * ** * Peak Number 9 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.16 ug/L 139053 Phenanthrene -dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyanocarbazole $$ 9H-Carbazole ... 192 C13H8N2 057102-93-9 64 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 3 6-Methoxy-2,4-dihydroxy-1,5-naph... 192 C9H8N203 000000-00-0 50 4 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 50 Abundance Scan 1656 (22.280 min): 00555.D (-) m/z 192.10 100.00% 192

5000

82 96 146 160 22.00 22.20 22.40 22.60

m/z-> 42 52 66 TrT ' . ' | H . r | ■ | I | | , ■ I I | I'' n । ■ 11. । ■■. 1.11377...... 'I'1 I'"I I'1'-'!' 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 JU m/z 96.10 15.02% Abundance #103424:3-Cyanocarbazo)e $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 22.00 22.20 22.40 22.60 96 164 m/ z 191.10 14.37% | 138

m/z-> 30 40 ' Ir ‘ ■11" 111 ■ TTTRPDT '' I ‘'1111' ■ I 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Ila Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 ......... M...... /1 22.00 22.20 22.40 22.60 5000 m/Z 193.10 14.07%

96 165 । .............. . .......................................... .. miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102277:6-Methoxy-2,4-dihydroxy-1,5-naphthyridine 192 22.00 22.20 22.40 22.60 m/Z 146.10 12.30%

5000 52 80 149 163 1 68 42 1 144 134 " I'1" I TT-p-n-rp-r * T’OIT | ....................A............. , '11 p ' 1 ' 1 I 1 ■ 1 ' i 1 ■ 1 ' i 1 ■ 1 1 i ' 1 ■ ' m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

0555.D SCAN508.M Wed Jan 30 09:01:52 2002 Page 11

NYC-WTC_000051545

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NYC-WTC_000051545Source: NYC Law Department, mirrored locally

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