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GCMS analysis results for sample AE00027, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.

NYC-WTC_000050735–000050753

Folder label: “GCMS X 1/4/02 A 1/25/02

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NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02JAN25\00027.D vial: 3 Acq On : 25 Jan 2002 4:47 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ************************************************************ * ******** Peak Number 2 Butanoic acid, methyl ester... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 3.60 0.14 ug/L 59635 1,4-Dichlorobenzene-d4 9.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 78 2 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 78 3 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 78 4 Butanoic acid, methyl ester 102 C5H10O2 000623-42-7 72 Abundance Scan 20 (3.602 min): 00027.D (-) m/z 43.10 100.00% 43 74

5000 59 87 AAAA 3.50 3.60 3.70 3.80 3.90 4.00 .............. 36 | || .51 , |..... | 1 ■ i ■ ' ' ■ i ■ ■ ■ 1 i 1 ■ ■ • i 1 « t । । < । ■ i ■ m/z 74.00 94.45% n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #9228: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 43 74

4 fi । pip m ।.... 111 nr ., । 5000 59 87 3.50 3.60 3.70 3.80 3.90 4.00 m/z71.10 68.06% 102 TTTTTTTTTTTTTETTTITIITI ' 1 1 1 1 ' 1 i ' ■ ■ ■ i 1 ' ' • i m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #9220: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 43 mRRR 74 3.50 3.60 3.70 3.80 3.90 4.00 15 m/z41.10 33.79% 5000 27 59 87 ■ ' i ' 1 1 ' I 33 1 1 1 ■ i ' ■ ■ ■ i I1' « I ' 1, । । ... . । i I ‘ * l * ' ' ' ( * > ■ • । 102 - • i m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #9227: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 43 74 A. ,. .... 3.50 3.60 3.70 3.80 3.90 4.00 m/z 87.10 31.34%

5000 59 87 — 69 ............ | 102 , +r TT— mpoag w m np m n ।। n/z-> 10 20 30 40 50 60 70 80 90 100 110 3.50 3.60 3.70 3.80 3.90 4.00

00027.D SCAN508.M Mon Jan 28 09:49:29 2002 Page 4

NYC-WTC_000050742

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NYC-WTC_000050742Source: NYC Law Department, mirrored locally

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