Laboratory report listing unknown compounds and surrogate recovery for sample AE00250 analyzed on January 28, 2002.
NYC-WTC_000050596–000050614Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C: \MSDCHEM\1\5973N\02JAN24\00250.D Vial: 6 Acq On : 24 Jan 2002 7:06 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 1 Butanoic acid, methyl ester... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 3.61 0.12 ug/L 58909 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 83 2 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 83 3 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 78 4 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 74 Abundance Scan 21 (3,613 min): 00250.D (-) m/z 43.10 100.00% 43 74
5000 59 87 ,41.4) 3.50 3.60 3.70 3.80 3.90 4.00
iz-> ll ... 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 i■ ' i1 ■" i ■ m/z 74.10 77.56% Abundance #9227: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 43 74
5000 ‘ 3.50 3.60 3.70 3.80 3.90 4.00 ' ‘ ‘ 59 87 m/z 71.10 67.86% Hmmpu i ■ ■" i • ■ 69 •11 tr PomogT ।j ■ । 102 ।j i miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #9228: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 43 74 ___________________ A_______ ■11' " ■ i • ■ ■ ■ i • ■ “ i ‘'1' i “ ■' i‘"' i 3.50 3.60 3.70 3.80 3.90 4.00 5000 m/z 41.10 37.70%
1.. 59 87
102 TTp-FTTpT-TTp-rrrp-rr ’ITT +t Pp Npgmmr mfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #9224: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... A 43 3.50 3.60 3.70 3.80 3.90 4.00 74 m/z 59.10 28.20% 5000 27 59 87 133 69 102 ''I'” ■ i ■ TTHE] Hmg Ir TTg ’t08311010011711112211’321’r"I1 miz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 3.50 3.60 3.70 3.80 3.90 4.00
)0250.D SCAN508.M Fri Jan 25 10:26:22 2002 Page 3
NYC-WTC_000050602
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NYC-WTC_000050481
Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050539
Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050519
Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050645
Laboratory report listing unknown compounds and surrogate recovery for sample AE00110 analyzed on February 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051549
Laboratory report showing GCMS analysis results for sample AE00556 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050735
Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006126
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03247 conducted on March 15, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050432
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050433
Fragmented page containing a document identifier and instructions regarding liquid-liquid extractor drip rates from January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050435
Gas chromatography-mass spectrometry calibration analysis of sample AE00167 detecting multiple organic compounds including nitrosamines and dichlorobenzenes.
Filed in the same folder
NYC-WTC_000050439
Laboratory report listing concentrations of volatile organic compounds in sample AE00167 analyzed on January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050444
Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.
Filed in the same folder